The estimation of the possibilities of synchrotron radiation X-ray fluorescent analysis and atomic spectrometry for the bone's elemental composition determination
Creators
- 1. Institute of Cytology and Genetics of the Siberian Branch of Russian Academy of Sciences, Acad. Kaptyug str., 2, Novosibirsk 630090 (Russian Federation)
- 2. United Institute of Geology, Geophysics and Mineralogy of the Siberian Branch of Russian Academy of Sciences, Novosibirsk 630090 (Russian Federation)
- 3. Novosibirsk State University (Russian Federation)
- 4. Nikolaev Institute of Inorganic Chemistry, Siberian Branch of RAS (Russian Federation)
Description
Possibilities of multielemental highly sensitive techniques of analysis have been studied: synchrotron radiation X-ray fluorescence analysis (SR XFA), and atomic emission spectrometry with inductively bound plasma (ISP) and atomic absorption spectrometry (AAS) with flame (air-acetylene) atomization for assay of element composition of bone tissue with minimal preparation procedure. Results of comparative studies of elemental composition of bone tissue samples from experimental animals with inherited accelerated aging (rats of OXYS strain) using the SR XFA, ISP and AAS techniques are presented. It is shown that there exists in principle a possibility of assay of 22 biologically important essential macro- and trace elements within the range of 1.0-100,000 μg/g with a mean square analysis error of no more them 10-15% when using SR XFA
Additional details
Identifiers
- DOI
- 10.1016/j.nima.2005.01.239;
- PII
- S0168-9002(05)00350-5;
Publishing Information
- Journal Title
- Nuclear Instruments and Methods in Physics Research. Section A, Accelerators, Spectrometers, Detectors and Associated Equipment
- Journal Volume
- 543
- Journal Issue
- 1
- Journal Page Range
- p. 271-273
- ISSN
- 0168-9002
- CODEN
- NIMAER
Conference
- Title
- 15. international synchrotron radiation conference
- Acronym
- SR 2004
- Dates
- 19-23 Jul 2004
- Place
- Novosibirsk (Russian Federation)
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 37033725
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- ABSORPTION; ABSORPTION SPECTROSCOPY; ACETYLENE; AIR; ATOMIZATION; AUGER ELECTRON SPECTROSCOPY; BONE TISSUES; EMISSION SPECTROSCOPY; ERRORS; FLAMES; MULTI-ELEMENT ANALYSIS; PLASMA; RATS; SKELETON; SYNCHROTRON RADIATION; TRACE AMOUNTS; X-RAY FLUORESCENCE ANALYSIS
- Descriptors DEC
- ALKYNES; ANIMAL TISSUES; ANIMALS; BODY; BREMSSTRAHLUNG; CHEMICAL ANALYSIS; CONNECTIVE TISSUE; ELECTROMAGNETIC RADIATION; ELECTRON SPECTROSCOPY; FLUIDS; GASES; HYDROCARBONS; MAMMALS; NONDESTRUCTIVE ANALYSIS; ORGANIC COMPOUNDS; ORGANS; RADIATIONS; RODENTS; SORPTION; SPECTROSCOPY; VERTEBRATES; X-RAY EMISSION ANALYSIS
Optional Information
- Copyright
- Copyright (c) 2005 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.