Published January 2006
| Version v1
Journal article
Facile conversion of [1-14C]lauronitrile to [1-14C]lauric acid under microwave irradiation
Creators
- 1. Immunoassay Labelled Compounds and Jonaki Board of Radiation and Isotope Technology, Navi Mumbai (India). Labelled Compounds
Description
A highly efficient and an optimized synthesis of [1-14C]lauric acid with high specific activity (50 mCi/mmol) is described. [1-14C]lauric acid was prepared from [1-14C]lauronitrile, in 2 minutes with a mixture of concentrated hydrochloric acid: propionic acid (1: 2 v/v) under microwave irradiation, in quantitative yield. (author)
Additional details
Publishing Information
- Journal Title
- Journal of Radioanalytical and Nuclear Chemistry
- Journal Volume
- 267
- Journal Issue
- 1
- Journal Page Range
- p. 245-246
- ISSN
- 0236-5731
- CODEN
- JRNCDM
INIS
- Country of Publication
- Hungary
- Country of Input or Organization
- Hungary
- INIS RN
- 37036330
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
- Descriptors DEI
- ACID HYDROLYSIS; CARBON 14; CHEMICAL PREPARATION; DODECANOIC ACID; HYDROCHLORIC ACID; MICROWAVE RADIATION; NITRILES; PROPIONIC ACID; RADIOPHARMACEUTICALS
- Descriptors DEC
- BETA DECAY RADIOISOTOPES; BETA-MINUS DECAY RADIOISOTOPES; CARBON ISOTOPES; CARBOXYLIC ACIDS; CHEMICAL REACTIONS; CHLORINE COMPOUNDS; DECOMPOSITION; DRUGS; ELECTROMAGNETIC RADIATION; EVEN-EVEN NUCLEI; HALOGEN COMPOUNDS; HYDROGEN COMPOUNDS; HYDROLYSIS; INORGANIC ACIDS; INORGANIC COMPOUNDS; ISOTOPES; LABELLED COMPOUNDS; LIGHT NUCLEI; LYSIS; MATERIALS; MONOCARBOXYLIC ACIDS; NUCLEI; ORGANIC ACIDS; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; RADIATIONS; RADIOACTIVE MATERIALS; RADIOISOTOPES; SOLVOLYSIS; SYNTHESIS; YEARS LIVING RADIOISOTOPES
Optional Information
- Notes
- 14 refs.