Published June 15, 1987 | Version v1
Journal article

The structure of trisodium-vanadate-trihydrate

  • 1. National Inst. for Researches in Inorganic Materials, Sakura, Ibaraki (Japan)

Description

Na3VO4.3H2O, Mr=237.95, trigonal, R3, a=8.5099(3), c=7.7876(3) A, V=488.40(4) A3, Z=3, Dx=2.427 Mg m-3, λ(CuKα1)=1.540562, λ(CuKα2)=1.544390 A for lattice parameters, λ(MoKα)=0.71073 A for intensity measurement, μ=1.59 mm-1, F(000)=354, T=298 K, final R=0.017 for 494 unique observed reflections. The O atoms and the water molecules are arranged like cubic close packing of spheres, the Na and the V atoms being situated in octahedral and tetrahedral interstices respectively. The NaO6 octahedra form a three-dimensional network through edge-sharing. The VO4 group shares its corners but no edges with these octahedra. (orig.)

Additional details

Additional titles

Original title (German)
Die Struktur des Trinatriumvanadattrihydrats

Publishing Information

Journal Title
Acta Crystallogr., Sect. C
Journal Volume
43
Journal Issue
6
Series
Acta Crystallogr., Sect. C.
Journal Page Range
1030-1032
ISSN
0108-2701
CODEN
ACSCE