Published 1993 | Version v1
Journal article

Synthesis of 14C-labeled Eschenmoser's salt: dimethyl([14C]methylene) ammonium iodide

  • 1. Texas Tech Univ., Lubbock, TX (United States). Dept. of Chemistry and Biochemistry

Description

A six step synthesis of dimethyl([14C]methylene)ammonium iodide (Eschenmoser's salt) is described. Sodium [2-14C]acetate was used as the starting material. The overall yield of the final product was 30% with specific activity 8 mCi/mol. (author)

Additional details

Publishing Information

Journal Title
Journal of Labelled Compounds and Radiopharmaceuticals
Journal Volume
33
Journal Issue
4
Journal Page Range
p. 301-304.
ISSN
0362-4803
CODEN
JLCRD4

INIS

Country of Publication
United Kingdom
Country of Input or Organization
United Kingdom
INIS RN
24071525
Subject category
S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
Descriptors DEI
CARBON 14 COMPOUNDS; CHEMICAL PREPARATION; LABELLING; ORGANIC NITROGEN COMPOUNDS
Descriptors DEC
CARBON COMPOUNDS; ORGANIC COMPOUNDS; SYNTHESIS