Exploration of synchrotron Mössbauer microscopy with micrometer resolution: forward and a new backscattering modality on natural samples
Creators
- 1. X-ray Sciences Division, Argonne National Laboratory, Argonne, IL 60439 (United States)
- 2. Department of Chemistry, University of California, Davis, CA 95616 (United States)
- 3. Center for Nanoscale Materials, Argonne National Laboratory, Argonne, IL 60439 (United States)
- 4. Biosciences Division, Argonne National Laboratory, Argonne, IL 60439 (United States)
- 5. Brown University, Providence, RI 02912 (United States)
- 6. Department of Earth and Planetary Sciences, American Museum of Natural History, New York, NY 10024 (United States)
- 7. Department of Chemistry, Fordham University, Bronx, NY 10458 (United States)
Description
New aspects of synchrotron Mössbauer microscopy have been reported, including micrometer spatial resolution, forward as well as backscattering geometry, and the ability to measure samples with natural isotopic abundance, such as meteorites. New aspects of synchrotron Mössbauer microscopy are presented. A 5 µm spatial resolution is achieved, and sub-micrometer resolution is envisioned. Two distinct and unique methods, synchrotron Mössbauer imaging and nuclear resonant incoherent X-ray imaging, are used to resolve spatial distribution of species that are chemically and magnetically distinct from one another. Proof-of-principle experiments were performed on enriched 57Fe phantoms, and on samples with natural isotopic abundance, such as meteorites
Availability note (English)
Available from http://dx.doi.org/10.1107/S0909049512032414; Available from http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3423314Additional details
Identifiers
- URL
- http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3423314;
- DOI
- 10.1107/S0909049512032414;
- PII
- S0909049512032414;
Publishing Information
- Journal Title
- Journal of Synchrotron Radiation
- Journal Volume
- 19
- Journal Issue
- Pt 5
- Journal Page Range
- p. 814-820
- ISSN
- 0909-0495
- CODEN
- JSYRES
INIS
- Country of Publication
- Denmark
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 47002112
- Subject category
- S62: RADIOLOGY AND NUCLEAR MEDICINE;
- Descriptors DEI
- BACKSCATTERING; BIOMEDICAL RADIOGRAPHY; EXPLORATION; IRON 57; METEORITES; MICROSCOPY; PHANTOMS; SPATIAL DISTRIBUTION; SPATIAL RESOLUTION; SYNCHROTRONS; X RADIATION
- Descriptors DEC
- ACCELERATORS; CYCLIC ACCELERATORS; DIAGNOSTIC TECHNIQUES; DISTRIBUTION; ELECTROMAGNETIC RADIATION; EVEN-ODD NUCLEI; INTERMEDIATE MASS NUCLEI; IONIZING RADIATIONS; IRON ISOTOPES; ISOTOPES; MEDICINE; MOCKUP; NUCLEAR MEDICINE; NUCLEI; RADIATIONS; RADIOLOGY; RESOLUTION; SCATTERING; STABLE ISOTOPES; STRUCTURAL MODELS
Optional Information
- Copyright
- Copyright (c) Lifen Yan et al. 2012
- Notes
- PMCID: PMC3423314; PMID: 22898962; PUBLISHER-ID: hf5209; OAI: oai:pubmedcentral.nih.gov:3423314; This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.