Published September 1, 2012 | Version v1
Journal article

Exploration of synchrotron Mössbauer microscopy with micrometer resolution: forward and a new backscattering modality on natural samples

  • 1. X-ray Sciences Division, Argonne National Laboratory, Argonne, IL 60439 (United States)
  • 2. Department of Chemistry, University of California, Davis, CA 95616 (United States)
  • 3. Center for Nanoscale Materials, Argonne National Laboratory, Argonne, IL 60439 (United States)
  • 4. Biosciences Division, Argonne National Laboratory, Argonne, IL 60439 (United States)
  • 5. Brown University, Providence, RI 02912 (United States)
  • 6. Department of Earth and Planetary Sciences, American Museum of Natural History, New York, NY 10024 (United States)
  • 7. Department of Chemistry, Fordham University, Bronx, NY 10458 (United States)

Description

New aspects of synchrotron Mössbauer microscopy have been reported, including micrometer spatial resolution, forward as well as backscattering geometry, and the ability to measure samples with natural isotopic abundance, such as meteorites. New aspects of synchrotron Mössbauer microscopy are presented. A 5 µm spatial resolution is achieved, and sub-micrometer resolution is envisioned. Two distinct and unique methods, synchrotron Mössbauer imaging and nuclear resonant incoherent X-ray imaging, are used to resolve spatial distribution of species that are chemically and magnetically distinct from one another. Proof-of-principle experiments were performed on enriched 57Fe phantoms, and on samples with natural isotopic abundance, such as meteorites

Availability note (English)

Available from http://dx.doi.org/10.1107/S0909049512032414; Available from http://www.ncbi.nlm.nih.gov/pmc/articles/PMC3423314

Additional details

Publishing Information

Journal Title
Journal of Synchrotron Radiation
Journal Volume
19
Journal Issue
Pt 5
Journal Page Range
p. 814-820
ISSN
0909-0495
CODEN
JSYRES

Optional Information

Copyright
Copyright (c) Lifen Yan et al. 2012
Notes
PMCID: PMC3423314; PMID: 22898962; PUBLISHER-ID: hf5209; OAI: oai:pubmedcentral.nih.gov:3423314; This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.