Published December 1982 | Version v1
Journal article

Synthesis of aluminium hexachloromolybdate and its interaction with some cyclic amines

  • 1. Bukharskij Tekhnologicheskij Inst. Pishchevoj i Legkoj Promyshlennosti (USSR)

Description

Aluminium hexachloromolybdate has been synthesized in concentrated hydrochloric acid by the reduction of Mo(5) and (6) compounds with atomic hydrogen (according to the reaction Al+HCl). Formation mechanism of AlMo3Cl6 is discussed. By means of ipteraction of AlMoCl6 with Py, An, Pipy in aqueous alcohol medium intrasubstituted amine complexes of Mo(3) of the type MoCl3A3 are prepared. According to IR absorption spectra a conclusion is drawn on the way of ligand coordination as to metal

Additional details

Additional titles

Original title (Russian)
Синтез гексахлоромолибдата алюминия и взаимодействие его с некоторыми циклическими аминами

Publishing Information

Journal Title
Zh. Obshch. Khim.
Journal Volume
52
Journal Issue
12
Series
Zh. Obshch. Khim.
Journal Page Range
2746-2751
ISSN
0044-460X

Optional Information

Notes
For English translation see the journal Journal of General Chemistry of the USSR (USA).