Synthesis of nickel oxide nanorods by Aloe vera leaf extract
Creators
- 1. University of Mazandaran, Department of Inorganic Chemistry, Faculty of Chemistry (Iran, Islamic Republic of)
Description
Nickel oxide nanorods were synthesized simply using Aloe vera extract solution and characterized by Fourier transform infrared spectroscopy and powder X-ray diffraction and the morphology of synthesized NiO nanorods were investigated by using of scanning electron microscopy technique. The electrochemical feature and specific capacitance of NiO nanorods were investigated by cyclic voltammetry method, and the results showed the high specific capacitance of NiO nanorods (about 1965 Fg−1). Also, the catalytic activity of NiO nanorods on the thermal decomposition of ammonium perchlorate (AP) was studied by differential scanning calorimetry and thermogravimetry analysis. The results indicated that addition of NiO nanorods increased the heat of decomposition of AP from 450 Jg−1 to 1450 Jg−1 and decreased the temperature of high-temperature decomposition step from 420 °C to about 351 °C. Also, the rate constant (k) enhanced from 5.7(± 0.2) × 10−3 to 1.4(± 0.2) × 10−2 s−1 in the presence of NiO nanorods via catalytic path.
Additional details
Identifiers
Publishing Information
- Journal Title
- Journal of Thermal Analysis and Calorimetry
- Journal Volume
- 136
- Journal Issue
- 2
- Journal Page Range
- p. 913-923
- ISSN
- 1388-6150
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 51086334
- Subject category
- S77: NANOSCIENCE AND NANOTECHNOLOGY;
- Descriptors DEI
- AMMONIUM PERCHLORATES; CALORIMETRY; CAPACITANCE; FOURIER TRANSFORM SPECTROMETERS; MORPHOLOGY; NANOSTRUCTURES; NICKEL OXIDES; POWDERS; PYROLYSIS; SCANNING ELECTRON MICROSCOPY; SOLUTIONS; THERMAL GRAVIMETRIC ANALYSIS; VOLTAMETRY; X-RAY DIFFRACTION
- Descriptors DEC
- AMMONIUM COMPOUNDS; CHALCOGENIDES; CHEMICAL ANALYSIS; CHEMICAL REACTIONS; CHLORINE COMPOUNDS; COHERENT SCATTERING; DECOMPOSITION; DIFFRACTION; DISPERSIONS; ELECTRICAL PROPERTIES; ELECTRON MICROSCOPY; GRAVIMETRIC ANALYSIS; HALOGEN COMPOUNDS; HOMOGENEOUS MIXTURES; MEASURING INSTRUMENTS; MICROSCOPY; MIXTURES; NICKEL COMPOUNDS; OXIDES; OXYGEN COMPOUNDS; PERCHLORATES; PHYSICAL PROPERTIES; QUANTITATIVE CHEMICAL ANALYSIS; SCATTERING; SPECTROMETERS; THERMAL ANALYSIS; THERMOCHEMICAL PROCESSES; TRANSITION ELEMENT COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2019 Akademiai Kiado, Budapest, Hungary