Bragg coherent x-ray diffractive imaging of a single indium phosphide nanowire
Creators
- 1. Deutsches Elektronen-Synchrotron DESY, Notkestraße 85, D-22607 Hamburg (Germany)
- 2. Niels Bohr Institute, University of Copenhagen, DK-2100 Copenhagen (Denmark)
- 3. Institut für Chemie, Universität Potsdam, Karl-Liebknecht-Strae 24-25, D-14476 Potsdam (Germany)
- 4. European XFEL GmbH, Albert-Einstein-Ring 19, D-22761, Hamburg (Germany)
- 5. Institute of Structural Physics, Technische Universität Dresden, D-01062 Dresden (Germany)
- 6. Synchrotron Radiation Research, Lund University, SE-22100 Lund (Sweden)
- 7. Department of Physics, University of California, San Diego, La Jolla, CA 92093 (United States)
- 8. Center for Free-Electron Laser Science CFEL, Notkestraße 85, D-22607 Hamburg (Germany)
- 9. Solid State Physics, Lund University, SE-22100 Lund (Sweden)
Description
Three-dimensional (3D) Bragg coherent x-ray diffractive imaging (CXDI) with a nanofocused beam was applied to quantitatively map the internal strain field of a single indium phosphide nanowire. The quantitative values of the strain were obtained by pre-characterization of the beam profile with transmission ptychography on a test sample. Our measurements revealed the 3D strain distribution in a region of 150 nm below the catalyst Au particle. We observed a slight gradient of the strain in the range of ±0.6% along the [111] growth direction of the nanowire. We also determined the spatial resolution in our measurements to be about 10 nm in the direction perpendicular to the facets of the nanowire. The CXDI measurements were compared with the finite element method simulations and show a good agreement with our experimental results. The proposed approach can become an effective tool for in operando studies of the nanowires. (paper)
Availability note (English)
Available from http://dx.doi.org/10.1088/2040-8978/18/6/064007Additional details
Identifiers
Publishing Information
- Journal Title
- Journal of Optics (Online)
- Journal Volume
- 18
- Journal Issue
- 6
- Journal Page Range
- [10 p.]
- ISSN
- 2040-8986
INIS
- Country of Publication
- United Kingdom
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 49059608
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- BEAM PROFILES; BRAGG REFLECTION; CATALYSTS; CRYSTAL GROWTH; FINITE ELEMENT METHOD; GOLD; INDIUM PHOSPHIDES; NANOWIRES; SPATIAL RESOLUTION; STRAINS; THREE-DIMENSIONAL LATTICES; X-RAY DIFFRACTION
- Descriptors DEC
- CALCULATION METHODS; COHERENT SCATTERING; CRYSTAL LATTICES; CRYSTAL STRUCTURE; DIFFRACTION; ELEMENTS; INDIUM COMPOUNDS; MATHEMATICAL SOLUTIONS; METALS; NANOSTRUCTURES; NUMERICAL SOLUTION; PHOSPHIDES; PHOSPHORUS COMPOUNDS; PNICTIDES; REFLECTION; RESOLUTION; SCATTERING; TRANSITION ELEMENTS