Published November 1992 | Version v1
Journal article

Solvent extraction of uranium (VI), thorium (IV) with petroleum sulfoxides (PSO)

  • 1. Dept. of Nuclear Science, Fudan Univ., Shanghai (China)
  • 2. Dept. of Chemistry, Tongji Univ., Shanghai (China)

Description

The influence of the temperature, as well as the concentrations of nitric acid, petroleum sulfoxides (PSO), salting-out agent and metal ions on the distribution ratio of uranium (VI), thorium (IV) has been systematically studied. It is found that the extraction regularity of PSO is similar to that of DOSO and TBP. Both uranium (VI) and thorium (IV) exhibit the maximum distribution ratios at 5-6 mol/l HNO3 and 3-4 mol/l HNO3, respectively. The extracted compounds are determined to be UO2(NO3)2 · 2PSO and Th(NO3)4 · 3PSO, respectively. The distribution ratios of uranium (VI) and thorium (IV) increase rapidly in the presence of salting-out agent. The extraction enthalpies of uranium (VI) and thorium (IV) with PSO are ΔHu = -26 kJ/mol and ΔHTh = -29 kJ/mol

Additional details

Publishing Information

Journal Title
Journal of Nuclear and Radiochemistry
Journal Volume
14
Journal Issue
4
Journal Page Range
p. 226-231.
ISSN
0253-9950
CODEN
HHHHDH