Published November 1989 | Version v1
Report Restricted

Standardization of a sulfur quantitative analysis method by X ray fluorescence in a leaching solution for bio-available sulfates in soil

  • 1. Seccion Industrial, Direccion General de Energia Nuclear, (Guatemala)

Description

A method for bio-available sulfate analysis in soils is described. A Ca(H2PO4) leaching solution was used for soil samples treatment. A standard NaSO4 solution was used for preparing a calibration curve and also the fundamental parameters method approach was employed. An Am-241 (100 mCi) source and a Si-Li detector were employed. Analysis could be done in 5 minutes; good reproducibility, 5 and accuracy, 5 were obtained. The method is very competitive with conventional nephelometry where good and reproducible suspensions are difficult to obtain. (author)

Availability note (English)

MF available from INIS under the Report Number.

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Additional details

Additional titles

Original title (Spanish)
Estandarizacion de un metodo de cuantificacion de azufre por fluorescencia de rayos X, en una solucion extractora de sulfato disponible en suelo

Publishing Information

Imprint Pagination
13 p.
Report number
DGEN-SI--2

INIS

Country of Publication
Guatemala
Country of Input or Organization
Guatemala
INIS RN
21034712
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
SOILS; SULFATES; X-RAY FLUORESCENCE ANALYSIS
Descriptors DEC
CHEMICAL ANALYSIS; NONDESTRUCTIVE ANALYSIS; OXYGEN COMPOUNDS; SULFUR COMPOUNDS; X-RAY EMISSION ANALYSIS