Advances in determination methods of 241Am in urine samples
Creators
- 1. China Institute of Atomic Energy, P.O. Box 275(15), Beijing (China)
Description
241Am is one of the most toxic transuranic nuclides due to its long half-life and α-particle emission, which needs to be surveilled in both internal individual exposure routine monitoring for workers and emergency rapid analysis. This paper aims to critically review some aspects of determination of 241Am in the urine sample. A typical radiochemical analysis procedure consists of calcium phosphate or oxalate co-precipitation, extraction chromatography with DGA or TRU resin, source preparation by electrodeposition in ammonium sulfate or oxalate or micro co-precipitation with Nd/CeF3. Newly progress in the measurement techniques of 241Am in urine, especially the capabilities of various mass spectrometry including radioactivity measuring instruments like alpha spectrometry, liquid scintillation spectrometry and gamma spectrometry or non-radioactive measuring instruments like mass spectrometry (ICP-MS, AMS etc.) has also been mentioned in this review. (authors)
Additional details
Identifiers
Publishing Information
- Journal Title
- Journal of Nuclear and Radiochemistry
- Journal Volume
- 42
- Journal Issue
- 1
- Journal Page Range
- p. 13-21
- ISSN
- 0253-9950
INIS
- Country of Publication
- China
- Country of Input or Organization
- China
- INIS RN
- 55094750
- Subject category
- S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
- Descriptors DEI
- AMERICIUM 241; AMMONIUM SULFATES; CALCIUM PHOSPHATES; COPRECIPITATION; EXTRACTION CHROMATOGRAPHY; GAMMA SPECTROSCOPY; ICP MASS SPECTROSCOPY; OXALATES; RADIOCHEMICAL ANALYSIS; REVIEWS; URINE
- Descriptors DEC
- ACTINIDE NUCLEI; ALKALINE EARTH METAL COMPOUNDS; ALPHA DECAY RADIOISOTOPES; AMERICIUM ISOTOPES; AMMONIUM COMPOUNDS; BIOLOGICAL MATERIALS; BIOLOGICAL WASTES; BODY FLUIDS; CALCIUM COMPOUNDS; CARBOXYLIC ACID SALTS; CHEMICAL ANALYSIS; CHROMATOGRAPHY; DOCUMENT TYPES; HEAVY NUCLEI; ISOTOPES; MASS SPECTROSCOPY; MATERIALS; NUCLEI; ODD-EVEN NUCLEI; OXYGEN COMPOUNDS; PHOSPHATES; PHOSPHORUS COMPOUNDS; PRECIPITATION; QUANTITATIVE CHEMICAL ANALYSIS; RADIOISOTOPES; SEPARATION PROCESSES; SPECTROSCOPY; SPONTANEOUS FISSION RADIOISOTOPES; SULFATES; SULFUR COMPOUNDS; WASTES; YEARS LIVING RADIOISOTOPES
Optional Information
- Notes
- 1 fig., 2 tabs., 42 refs.; http://dx.doi.org/10.7538/hhx.2019.YX.2018067