Published November 1992 | Version v1
Journal article

(η1-Cp) Tc(NAr)3: Synthesis and structure

  • 1. Los Alamos National Laboratory, NM (United States)

Description

The reaction of KCp with TcI(NAr)3 (Ar = 2,6-diisopropylphenyl) rapidly forms (η1-Cp)Tc(NAr)3. A single-crystal X-ray determination confirmed the η1 nature of the cyclopentadienyl ligand. When TcI(NAr)3 is treated with an excess of KCp, a second cyclopentadienyl group is added to the metal, giving K[Cp2Tc(NAr)3]. 12 refs., 1 fig

Additional details

Publishing Information

Journal Title
Organometallics
Journal Volume
11
Journal Issue
11
Journal Page Range
p. 3501-3503.
ISSN
0276-7333
CODEN
ORGND7

INIS

Country of Publication
United States
Country of Input or Organization
United States
INIS RN
28017110
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Descriptors DEI
CHEMICAL PREPARATION; ORGANOMETALLIC COMPOUNDS; STRUCTURAL CHEMICAL ANALYSIS; TECHNETIUM COMPLEXES
Descriptors DEC
COMPLEXES; ORGANIC COMPOUNDS; SYNTHESIS; TRANSITION ELEMENT COMPLEXES