Published November 1991 | Version v1
Journal article

Synthesis of (E)- and (Z)-2,3-bis (trifluoromethyl) allyl alcohols by γ-ray irradiation of hexafluoro-2-butyne with alcohols and some reactions

  • 1. Government Industrial Research Inst., Nagoya (Japan)

Description

Radiation-induced addition reaction of alcohols to hexafluoro-2-butyne provided (E)-and (Z)-2,3-bis (trifluoromethyl) allyl alcohols, which were dehydrated to afford 1,2-bis (trifluoromethyl)-1,3-butadienes. Thermal cyclization of 3-methyl-1,2-bis (trifluoromethyl)-1,3-butadiene afforded 1-methyl-2,3-bis (trifluoromethyl) cyclobutene. (author)

Additional details

Publishing Information

Journal Title
Bulletin of the Chemical Society of Japan
Journal Volume
64
Journal Issue
11
Series
Bull. Chem. Soc. Jpn.
Journal Page Range
3494-3496
ISSN
0009-2673
CODEN
BCSJA