Microstructural characterization by electron backscatter diffraction of a hot worked Al-Cu-Mg alloy
- 1. Department of Physical Metallurgy, CENIM, CSIC, Av. Gregorio del Amo 8, 28040 Madrid (Spain)
Description
Research highlights: → The most favourable conditions for hot workability have been determined. → EBSD was employed to characterize the obtained microtexture and microstructure. → The Al 2024 alloy torsion tested at 408 deg. C and 2.1 s-1 showed maximum ductility. → Solid solution and fine precipitates favour a fine microstructure at 408 deg. C. → The increase in test temperature to 467 deg. C produces a sharp decrease in ductility. - Abstract: Hot torsion tests to fracture to simulate thermomechanical processing were carried out on a solution-treated Al-Cu-Mg alloy (Al 2024-T351) at constant temperature. Torsion tests were conducted in the range 278-467 deg. C, and at two strain rates, 2.1 and 4.5 s-1. Electron backscatter diffraction (EBSD) was employed to characterize the microtexture and microstructure before and after testing. The microstructural evolution during torsion deformation at different temperatures and strain rate conditions determines the mechanical properties at room temperature of the Al 2024 alloy since grain refining, dynamic precipitation and precipitate coalescence occur during the torsion test. These mechanical properties were measured by Vickers microhardness tests. At 408 deg. C and 2.1 s-1 the optimum combination of solid solution and incipient precipitation gives rise to maximum ductility and large fraction of fine and misoriented grains (fHAB = 54%). In contrast, the increase in test temperature to 467 deg. C produces a sharp decrease in ductility, attributed to the high proportion of alloying elements in solid solution. Both the stress-strain flow curves obtained by torsion tests and the final microstructures are a consequence of recovery phenomena and the dynamic nature of the precipitation process taking place during deformation.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.msea.2010.12.045Additional details
Identifiers
- DOI
- 10.1016/j.msea.2010.12.045;
- PII
- S0921-5093(10)01451-6;
Publishing Information
- Journal Title
- Materials Science and Engineering. A, Structural Materials: Properties, Microstructure and Processing
- Journal Volume
- 528
- Journal Issue
- 7-8
- Journal Page Range
- p. 3161-3168
- ISSN
- 0921-5093
- CODEN
- MSAPE3
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 44012954
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- ALUMINIUM ALLOYS; BACKSCATTERING; COALESCENCE; COPPER ALLOYS; DEFORMATION; DUCTILITY; ELECTRON DIFFRACTION; FRACTURES; MAGNESIUM ALLOYS; MATERIALS TESTING; MICROHARDNESS; MICROSTRUCTURE; PRECIPITATION; RECRYSTALLIZATION; SOLID SOLUTIONS; STRAIN RATE; STRAINS; STRESSES; TEMPERATURE DEPENDENCE; TORSION
- Descriptors DEC
- ALLOYS; COHERENT SCATTERING; DIFFRACTION; DISPERSIONS; FAILURES; HARDNESS; HOMOGENEOUS MIXTURES; MECHANICAL PROPERTIES; MIXTURES; SCATTERING; SEPARATION PROCESSES; SOLUTIONS; TENSILE PROPERTIES; TESTING; TRANSITION ELEMENT ALLOYS
Optional Information
- Copyright
- Copyright (c) 2010 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.