Published 1982 | Version v1
Miscellaneous

Determination of the radiochemical purity of tritium-labelled nucleoside-5'-triphosphates using PEI-cellulose microcolumns

  • 1. AN SSSR, Moscow. Inst. Molekulyarnoj Genetiki

Description

The radiochemical purity of tritium-labelled nucleoside-5'-triphosphates was analysed by means of a highly sensitive continuous-operation detector of UV absorption and a PEI-cellulose microcolumn (3 mm in diameter, 130 mm long). Analysis was performed with 0.1-0.2 nucleotide optical density units (lambda = 254 nm). Elution was carried out by a NaCl concentration gradient. All nucleotides were separated under identical conditions. The duration of analysis did not exceed 1-2 hrs

Additional details

Additional titles

Original title (Russian)
Определение радиохимической чистоты меченных тритием нуклеозид-5′-трифосфатов с применением микроколонок с ПЭИ-целлюлозой

Publishing Information

Imprint Title
Radioisotope-labelled organic compounds. Part 2
Journal Page Range
p. 266-270.
Report number
INIS-mf--10548

Conference

Title
Radioisotope-labelled organic compounds.
Dates
8-11 Dec 1981.
Place
Leningrad (USSR).

INIS

Country of Publication
International Centre for Scientific and Technical Information (ICSTI)
Country of Input or Organization
International Centre for Scientific and Technical Information (ICSTI)
INIS RN
18021892
Subject category
S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY; S63: RADIATION, THERMAL, AND OTHER ENVIRONMENTAL POLLUTANT EFFECTS ON LIVING ORGANISMS AND BIOLOGICAL MATERIALS;
Resource subtype / Literary indicator
Conference
Descriptors DEI
CELLULOSE; IMPURITIES; ION EXCHANGE CHROMATOGRAPHY; LEACHING; NUCLEOTIDES; OPACITY; ORGANIC PHOSPHORUS COMPOUNDS; RADIOACTIVITY; SENSITIVITY; TRITIUM COMPOUNDS
Descriptors DEC
CARBOHYDRATES; CHROMATOGRAPHY; DISSOLUTION; HYDROGEN COMPOUNDS; OPTICAL PROPERTIES; ORGANIC COMPOUNDS; PHYSICAL PROPERTIES; POLYSACCHARIDES; SACCHARIDES; SEPARATION PROCESSES

Optional Information

Notes
3 figs.; 6 refs. Imprint:Organicheskie soedineniya, mechennye radioaktivnymi izotopami.;Materialy 2 Simpoziuma stran-chlenov SEhV, Leningrad, 8-11 dekabrya 1981 g. Chast' 2.