Stress induced martensite variants revealed by in situ high resolution electron backscatter diffraction (HR-EBSD)
- 1. Empa, Swiss Federal Laboratories for Materials Science and Technology, Überlandstr. 129, Dübendorf 8600 (Switzerland)
- 2. Henry Moseley X-ray Imaging Facility, University of Manchester, Alan Turing Building, Manchester M13 9PL (United Kingdom)
- 3. Empa, Swiss Federal Laboratories for Materials Science and Technology, Feuerwerkerstrasse 39, Thun 3602 (Switzerland)
Description
Highlights: • In situ HR-EBSD was done to correlate stress induced phase transformation and stress fields. • A Schmid factor analysis was extended by the analysis of local resolved shear stresses. • Growth of an unexpected martensite variant near the grain boundary is observed. • Stress concentrations are shown to trigger the growth of the unexpected variant. In situ HR-EBSD during FeMnSi-based micro-pillar compression is used to correlate phase transformations and its underlying stresses. A simple experimental configuration containing two grains, one grain boundary and a uniaxial compression causes complex stress fields. Two out of three differently orientated stress induced martensite variants are expected to form due to high Schmid factors. To reveal the origin of growth of the third variant with a low Schmid factor, we calculate global stress maps and local resolved shear stress maps based on HR-EBSD measurements. Localized shear stresses at the grain boundary are identified to cause the growth of the not expected near grain boundary variant.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.matdes.2018.04.006Additional details
Identifiers
- DOI
- 10.1016/j.matdes.2018.04.006;
- PII
- S0264127518302685;
Publishing Information
- Journal Title
- Materials and Design
- Journal Volume
- 151
- Journal Page Range
- p. 83-88
- ISSN
- 0264-1275
- CODEN
- MADSD2
INIS
- Country of Publication
- United Kingdom
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 53005618
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- BACKSCATTERING; COMPRESSION; ELECTRON DIFFRACTION; GRAIN BOUNDARIES; MARTENSITE; PHASE TRANSFORMATIONS; RESOLUTION; SHEAR; STRESSES
- Descriptors DEC
- ALLOYS; CARBON ADDITIONS; COHERENT SCATTERING; DIFFRACTION; IRON ALLOYS; MICROSTRUCTURE; SCATTERING; TRANSITION ELEMENT ALLOYS
Optional Information
- Copyright
- Copyright (c) 2018 Elsevier Ltd. All rights reserved.