Published August 2018 | Version v1
Journal article

Stress induced martensite variants revealed by in situ high resolution electron backscatter diffraction (HR-EBSD)

  • 1. Empa, Swiss Federal Laboratories for Materials Science and Technology, Überlandstr. 129, Dübendorf 8600 (Switzerland)
  • 2. Henry Moseley X-ray Imaging Facility, University of Manchester, Alan Turing Building, Manchester M13 9PL (United Kingdom)
  • 3. Empa, Swiss Federal Laboratories for Materials Science and Technology, Feuerwerkerstrasse 39, Thun 3602 (Switzerland)

Description

Highlights: • In situ HR-EBSD was done to correlate stress induced phase transformation and stress fields. • A Schmid factor analysis was extended by the analysis of local resolved shear stresses. • Growth of an unexpected martensite variant near the grain boundary is observed. • Stress concentrations are shown to trigger the growth of the unexpected variant. In situ HR-EBSD during FeMnSi-based micro-pillar compression is used to correlate phase transformations and its underlying stresses. A simple experimental configuration containing two grains, one grain boundary and a uniaxial compression causes complex stress fields. Two out of three differently orientated stress induced martensite variants are expected to form due to high Schmid factors. To reveal the origin of growth of the third variant with a low Schmid factor, we calculate global stress maps and local resolved shear stress maps based on HR-EBSD measurements. Localized shear stresses at the grain boundary are identified to cause the growth of the not expected near grain boundary variant.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matdes.2018.04.006

Additional details

Identifiers

DOI
10.1016/j.matdes.2018.04.006;
PII
S0264127518302685;

Publishing Information

Journal Title
Materials and Design
Journal Volume
151
Journal Page Range
p. 83-88
ISSN
0264-1275
CODEN
MADSD2

INIS

Country of Publication
United Kingdom
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
53005618
Subject category
S36: MATERIALS SCIENCE;
Descriptors DEI
BACKSCATTERING; COMPRESSION; ELECTRON DIFFRACTION; GRAIN BOUNDARIES; MARTENSITE; PHASE TRANSFORMATIONS; RESOLUTION; SHEAR; STRESSES
Descriptors DEC
ALLOYS; CARBON ADDITIONS; COHERENT SCATTERING; DIFFRACTION; IRON ALLOYS; MICROSTRUCTURE; SCATTERING; TRANSITION ELEMENT ALLOYS

Optional Information

Copyright
Copyright (c) 2018 Elsevier Ltd. All rights reserved.