Determination of hard-measurable radionuclide in samples of radioactive waste from decommissioned NPP V1
- 1. Univerzita Komenskeho, Prirodovedeckd fakulta, Katedra jadrovej chemie, 84215 Bratislava (Slovakia)
Description
The paper describes a simple distillation method for the determination of 129? by liquid scintillation spectrometry. The chemical yields of separation by gravimetric determination of iodine as PdI2-H2O were determined. For testing of the method a suitable apparatus for distillation of iodine was designed. The optimum conditions for the effective distillation of iodine was nitric acid in concentration range of (1 - 2) mol·dm3 with 0.4 g of NaNO2 as iodide oxidizing agent (I- -> I2). The optimum time for coagulation of PdI2-H2O precipitate was 24 hours and distillation time was only 20 minutes. Optimized method for the determination of 129I for real samples from nuclear power plant V1 in Jaslovske Bohunice was applied. 129I by liquid scintillation counter TriCarb 3100TR with high detection efficiency (95 %) was measured. (authors)
Additional details
Additional titles
- Original title (Slovak)
- Stanovenie tazko-meratelneho radionuklidu v RAO z vyradenej JE VI
Identifiers
Publishing Information
- Publisher
- Vydavatelstvo Univerzity Komenskeho
- Imprint Place
- Bratislava (Slovakia)
- ISBN
- 978-80-223-4103-5
- Imprint Title
- Student Scientific Conference PriF UK 2016. Proceedings of reviewed contributions
- Imprint Pagination
- 1602 p.
- Journal Page Range
- p. 937-941
- Report number
- INIS-SK--2016-041
Conference
- Title
- Student Scientific Conference PriF UK 2016
- Original Conference Title
- Studentska vedecka konferencia PriF UK 2016
- Dates
- 27 Apr 2016
- Place
- Bratislava (Slovakia)
INIS
- Country of Publication
- Slovakia
- Country of Input or Organization
- Slovakia
- INIS RN
- 47082812
- Subject category
- S12: MANAGEMENT OF RADIOACTIVE WASTES, AND NON-RADIOACTIVE WASTES FROM NUCLEAR FACILITIES; S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
- Resource subtype / Literary indicator
- Conference, Numerical Data
- Descriptors DEI
- DISTILLATION; DISTILLATION EQUIPMENT; EXPERIMENTAL DATA; IODINE 129; LIQUID SCINTILLATION DETECTORS; NUCLEAR CHEMISTRY; RADIOACTIVE WASTE MANAGEMENT; RADIOACTIVE WASTES; RADIOCHEMICAL ANALYSIS; X-RAY DETECTION
- Descriptors DEC
- BETA DECAY RADIOISOTOPES; BETA-MINUS DECAY RADIOISOTOPES; CHEMICAL ANALYSIS; CHEMISTRY; DATA; DETECTION; EQUIPMENT; INFORMATION; INTERMEDIATE MASS NUCLEI; INTERNAL CONVERSION RADIOISOTOPES; IODINE ISOTOPES; ISOTOPES; MANAGEMENT; MATERIALS; MEASURING INSTRUMENTS; NUCLEI; NUMERICAL DATA; ODD-EVEN NUCLEI; QUANTITATIVE CHEMICAL ANALYSIS; RADIATION DETECTION; RADIATION DETECTORS; RADIOACTIVE MATERIALS; RADIOISOTOPES; SCINTILLATION COUNTERS; SEPARATION PROCESSES; WASTE MANAGEMENT; WASTES; YEARS LIVING RADIOISOTOPES
Optional Information
- Notes
- 1 tab., 1 fig., 10 refs. Imprint:Published on CDROM 58.6 MBytes in PDF format;Studentska vedecka konferencia PriF UK 2016. Zbornik recenzovanych prispevkov