Published March 2005
| Version v1
Journal article
Preparation of hollow carbon nanospheres at low temperature via new reaction route
- 1. Auhui Key Laboratory of Functional Molecular Solids, College of Chemistry and Materials Science, Anhui Normal University, Number 1, Beijing East Road, Wuhu City, Anhui province 241000 (China)
Description
Hollow carbon nanospheres were obtained at 200oC via a new reaction route, by using magnesium, hexachloroethane and aluminum trichloride as starting materials and benzene as solvent. The products were characterized with X-ray diffraction pattern, transmission electron microscope, high-resolution transmission electron microscope images and Raman spectrum. The reaction conditions are easy to be maintained and controlled. They may provide a new method to produce other carbonaceous materials. A possible mechanism of reaction was proposed
Additional details
Identifiers
- DOI
- 10.1016/j.jssc.2004.12.008;
- PII
- S0022-4596(04)00647-4;
Publishing Information
- Journal Title
- Journal of Solid State Chemistry
- Journal Volume
- 178
- Journal Issue
- 3
- Journal Page Range
- p. 908-911
- ISSN
- 0022-4596
- CODEN
- JSSCBI
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 37037297
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- ALUMINIUM CHLORIDES; CARBON; CARBONACEOUS MATERIALS; GRIGNARD REAGENTS; MAGNESIUM; NANOSTRUCTURES; RAMAN SPECTRA; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION
- Descriptors DEC
- ALKALINE EARTH METAL COMPOUNDS; ALKALINE EARTH METALS; ALUMINIUM COMPOUNDS; CHLORIDES; CHLORINE COMPOUNDS; COHERENT SCATTERING; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTS; HALIDES; HALOGEN COMPOUNDS; MAGNESIUM COMPOUNDS; MATERIALS; METALS; MICROSCOPY; NONMETALS; ORGANIC COMPOUNDS; ORGANOMETALLIC COMPOUNDS; SCATTERING; SPECTRA
Optional Information
- Copyright
- Copyright (c) 2004 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.