Published November 1984 | Version v1
Journal article

Lanthanide chelates of fluorinated β-diketones. Pt. 3

  • 1. New South Wales Univ., Kensington (Australia). School of Chemistry

Description

The mass spectra of sixty lanthanide chelates of the fluorinated β-diketones RC(OH)=CHCOCF3 (R = 2-theonyl, p-BrC6H4, m-MeC6H4, o-MeC6H4, and Bu-t) have been obtained. The mass spectra were essentially similar, in contrast to those found for d-block transition metal chelates. Valency change from 3 to 2 occurred with samarium (4f5), europium (4f6), thulium (4f12), and ytterbium (4f13); the intensity of the Met(II)-containing peaks varied: Eu >> Sm > Yb > Tm, reflecting the decreasing tendency of these lanthanides to display bivalency. Valency change from 4 to 3 was observed with cerium (4f1) but not with terbium (4f8). (orig.)

Additional details

Additional titles

Subtitle (English)
Mass spectra of lanthanide chelates of five fluorinated #beta#-diketones

Publishing Information

Journal Title
Transition Met. Chem.
Journal Volume
9
Journal Issue
11
Series
CODEN: TMCHD.;Transition Met. Chem.
Journal Page Range
433-438
ISSN
0340-4285