Published January 2013 | Version v1
Journal article

Status report on sample preparation facilities for 14C analysis at the new CologneAMS center

  • 1. Institute of Geology and Mineralogy, University of Cologne, 50674 Cologne (Germany)
  • 2. Ion Beam Physics, ETH Zürich, 8093 Zürich (Switzerland)
  • 3. Institute of Nuclear Physics, University of Cologne, 50674 Cologne (Germany)

Description

The new AMS facility at University of Cologne (CologneAMS), Germany, was established in 2010 with the delivery of the HVE 6 MV Tandetron AMS, which will be used for 14C, 26Al, 36Cl, 41Ca, 129I, 239U and 244Pu analyses. Parallel to the AMS installation the radiocarbon group has started to set up and test sample preparation methods and instruments for different materials. We present first results of reference and standard materials that have been processed and graphitized in our lab and measured at the ETH and CologneAMS facilities. The graphitization blank and its influence on small samples sizes processed with an automated graphitization system have been determined. Work on isolation of individual organic compounds with a preparative gas chromatography system has been started. The focus of our future work will be on reducing process blank levels and sample sizes as well as on the application of compound-specific radiocarbon analyses in (paleo-) environmental research.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.nimb.2012.02.012

Additional details

Identifiers

DOI
10.1016/j.nimb.2012.02.012;
PII
S0168-583X(12)00105-X;

Publishing Information

Journal Title
Nuclear Instruments and Methods in Physics Research. Section B, Beam Interactions with Materials and Atoms
Journal Volume
294
Journal Page Range
p. 168-172
ISSN
0168-583X
CODEN
NIMBEU

Conference

Title
12. international conference on accelerator mass spectrometry
Dates
20-25 Mar 2011
Place
Wellington (New Zealand)

Optional Information

Copyright
Copyright (c) 2012 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.