Status report on sample preparation facilities for 14C analysis at the new CologneAMS center
Creators
- 1. Institute of Geology and Mineralogy, University of Cologne, 50674 Cologne (Germany)
- 2. Ion Beam Physics, ETH Zürich, 8093 Zürich (Switzerland)
- 3. Institute of Nuclear Physics, University of Cologne, 50674 Cologne (Germany)
Description
The new AMS facility at University of Cologne (CologneAMS), Germany, was established in 2010 with the delivery of the HVE 6 MV Tandetron AMS, which will be used for 14C, 26Al, 36Cl, 41Ca, 129I, 239U and 244Pu analyses. Parallel to the AMS installation the radiocarbon group has started to set up and test sample preparation methods and instruments for different materials. We present first results of reference and standard materials that have been processed and graphitized in our lab and measured at the ETH and CologneAMS facilities. The graphitization blank and its influence on small samples sizes processed with an automated graphitization system have been determined. Work on isolation of individual organic compounds with a preparative gas chromatography system has been started. The focus of our future work will be on reducing process blank levels and sample sizes as well as on the application of compound-specific radiocarbon analyses in (paleo-) environmental research.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.nimb.2012.02.012Additional details
Identifiers
- DOI
- 10.1016/j.nimb.2012.02.012;
- PII
- S0168-583X(12)00105-X;
Publishing Information
- Journal Title
- Nuclear Instruments and Methods in Physics Research. Section B, Beam Interactions with Materials and Atoms
- Journal Volume
- 294
- Journal Page Range
- p. 168-172
- ISSN
- 0168-583X
- CODEN
- NIMBEU
Conference
- Title
- 12. international conference on accelerator mass spectrometry
- Dates
- 20-25 Mar 2011
- Place
- Wellington (New Zealand)
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 44084971
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- ALUMINIUM 26; CALCIUM 41; CARBON 14; CHLORINE 36; GAS CHROMATOGRAPHY; GRAPHITIZATION; IODINE 129; MASS SPECTROSCOPY; ORGANIC COMPOUNDS; PLUTONIUM 244; SAMPLE PREPARATION; TANDEM ELECTROSTATIC ACCELERATORS; URANIUM 239
- Descriptors DEC
- ACCELERATORS; ACTINIDE NUCLEI; ALKALINE EARTH ISOTOPES; ALPHA DECAY RADIOISOTOPES; ALUMINIUM ISOTOPES; BETA DECAY RADIOISOTOPES; BETA-MINUS DECAY RADIOISOTOPES; BETA-PLUS DECAY RADIOISOTOPES; CALCIUM ISOTOPES; CARBON ISOTOPES; CHLORINE ISOTOPES; CHROMATOGRAPHY; ELECTRON CAPTURE RADIOISOTOPES; ELECTROSTATIC ACCELERATORS; EVEN-EVEN NUCLEI; EVEN-ODD NUCLEI; HEAVY NUCLEI; INTERMEDIATE MASS NUCLEI; INTERNAL CONVERSION RADIOISOTOPES; IODINE ISOTOPES; ISOTOPES; LIGHT NUCLEI; MINUTES LIVING RADIOISOTOPES; NUCLEI; ODD-EVEN NUCLEI; ODD-ODD NUCLEI; PLUTONIUM ISOTOPES; RADIOISOTOPES; SECONDS LIVING RADIOISOTOPES; SEPARATION PROCESSES; SPECTROSCOPY; SPONTANEOUS FISSION RADIOISOTOPES; URANIUM ISOTOPES; YEARS LIVING RADIOISOTOPES
Optional Information
- Copyright
- Copyright (c) 2012 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.