Published June 2019
| Version v1
Journal article
Synthesis of 3,4-Dihydro-2H-[1,3]thiazino[3,2-c]quinazolinium Systems by Heterocyclization of 4-(Butenylsulfanyl)- and 4-(Cinnamylsulfanyl)qinazolines
- 1. South Ural State University (Russian Federation)
- 2. Perm State National Research University (Russian Federation)
Description
The alkylation of quinazoline-4(3H)-thione with 4-bromobut-1-ene and cinnamyl chloride gave previously unknown 4-(but-3-en-1-ylsulfanyl)- and 4-(cinnamylsulfanyl)quinazolines which reacted with iodine and bromine to afford 3,4-dihydro-2H-[1,3]thiazino[3,2-c]quinazolin-5-ium salts. The structure of the products was studied by GC/MS, 1H NMR, and X-ray analysis.
Additional details
Identifiers
Publishing Information
- Journal Title
- Russian Journal of Organic Chemistry
- Journal Volume
- 55
- Journal Issue
- 6
- Journal Page Range
- p. 748-754
- ISSN
- 1070-4280
INIS
- Country of Publication
- Russian Federation
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 51108702
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- ALKYLATION; BROMINE; CHLORIDES; GAS CHROMATOGRAPHY; HYDROGEN 1; IODINE; MASS SPECTROSCOPY; NUCLEAR MAGNETIC RESONANCE; SALTS; SYNTHESIS; X RADIATION
- Descriptors DEC
- CHEMICAL REACTIONS; CHLORINE COMPOUNDS; CHROMATOGRAPHY; ELECTROMAGNETIC RADIATION; ELEMENTS; HALIDES; HALOGEN COMPOUNDS; HALOGENS; HYDROGEN ISOTOPES; IONIZING RADIATIONS; ISOTOPES; LIGHT NUCLEI; MAGNETIC RESONANCE; NONMETALS; NUCLEI; ODD-EVEN NUCLEI; RADIATIONS; RESONANCE; SEPARATION PROCESSES; SPECTROSCOPY; STABLE ISOTOPES
Optional Information
- Copyright
- Copyright (c) 2019 Pleiades Publishing, Ltd.