Synthesis characterization rheological and morphological study of a new epoxy resin pentaglycidyl ether pentaphenoxy of phosphorus and their composite (PGEPPP/MDA/PN)
Creators
- 1. Ibn Tofail University, Laboratory of Agricultural Resources, Polymers and Process Engineering (LARPPE), Team of Polymer and Organic Chemistry (TPOC), Department of Chemistry, Faculty of Sciences (Morocco)
- 2. ESITH (Hight School of Textile and Clothing Industries), Laboratory REMTEX (Morocco)
- 3. Royal Naval School, University Department (Morocco)
Description
Our objective in this work consists in the synthesis, the characterization, the elaboration, the formulation, and the rheological study of the new phosphoric epoxy resin: pentaglycidyl ether pentaphenoxy of phosphorus (PGEPPP). Thus, we identified this polymer by Fourier transform infrared spectroscopy. Then, its chemical structure was confirmed by nuclear magnetic resonance of proton (1H NMR) and carbon (13C NMR). Furthermore, the rheological analyzes of the epoxy resin and their composite (PGEPPP/MDA/PN) were determined by the RHM01-RD HAAKE rheometer. Moreover, this epoxy polymer and their composite have been applied in flow phenomena and implementation. Finally, we proceeded to the morphological of the composite (PGEPPP/MDA/PN) using the scanning electron microscope, in order to confirm the dispersion of the natural phosphate load incorporated into the prepared composite.
Additional details
Identifiers
Publishing Information
- Journal Title
- Polymer Bulletin
- Journal Volume
- 76
- Journal Issue
- 9
- Journal Page Range
- p. 4859-4878
- ISSN
- 0170-0839
- CODEN
- POBUDR
INIS
- Country of Publication
- Germany
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 51103291
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- CARBON 13; EPOXIDES; ETHERS; FOURIER TRANSFORM SPECTROMETERS; HYDROGEN 1; INFRARED SPECTRA; NUCLEAR MAGNETIC RESONANCE; PHOSPHATES; PHOSPHORUS; PROTONS; RESINS; RHEOLOGY; SCANNING ELECTRON MICROSCOPY; SYNTHESIS
- Descriptors DEC
- BARYONS; CARBON ISOTOPES; ELECTRON MICROSCOPY; ELEMENTARY PARTICLES; ELEMENTS; EVEN-ODD NUCLEI; FERMIONS; HADRONS; HYDROGEN ISOTOPES; ISOTOPES; LIGHT NUCLEI; MAGNETIC RESONANCE; MEASURING INSTRUMENTS; MICROSCOPY; NONMETALS; NUCLEI; NUCLEONS; ODD-EVEN NUCLEI; ORGANIC COMPOUNDS; ORGANIC OXYGEN COMPOUNDS; ORGANIC POLYMERS; OXYGEN COMPOUNDS; PETROCHEMICALS; PETROLEUM PRODUCTS; PHOSPHORUS COMPOUNDS; POLYMERS; RESONANCE; SPECTRA; SPECTROMETERS; STABLE ISOTOPES
Optional Information
- Copyright
- Copyright (c) 2019 Springer-Verlag GmbH Germany, part of Springer Nature