Published July 2016 | Version v1
Journal article

Production of complex rubidium and cesium hydrogen sulfate‒phosphates

  • 1. Russian Academy of Sciences, Shubnikov Institute of Crystallography (Russian Federation)
  • 2. Lobachevsky State University of Nizhny Novgorod (Russian Federation)

Description

The solubility in the CsH2PO4‒CsHSO4‒H2O system at different temperatures (25, 50, and 75°C) is studied and the phase equilibria in the Rb3H(SO4)2‒RbH2PO4‒H2O system under isothermal conditions (at 25°C) are analyzed. The temperature and concentration conditions for forming Rb2(HSO4)(H2PO4), Rb4(HSO4)3(H2PO4), Cs4(HSO4)3(H2PO4), Cs3(HSO4)2(H2PO4), Cs2(HSO4)(H2PO4), and Cs6H(HSO4)3(H2PO4)4 compounds (the latter has been obtained for the first time) are determined. The conditions for growing large single crystals of complex acid rubidium and cesium salts are found.

Additional details

Identifiers

Publishing Information

Journal Title
Crystallography Reports
Journal Volume
61
Journal Issue
4
Journal Page Range
p. 675-681
ISSN
1063-7745
CODEN
CYSTE3

Optional Information

Copyright
Copyright (c) 2016 Pleiades Publishing, Inc.