Published September 2010 | Version v1
Journal article

Microwave sintering of β-SiAlON-ZrO2 composites

  • 1. New York State College of Ceramics, Alfred University, Alfred, NY 14802 (United States)

Description

Densification, phase transformation, microstructure evolution and hardness of microwave sintered β-SiAlON-ZrO2 composites were investigated and compared with conventionally sintered samples. Sintering trials were performed by a high vacuum capable 2.45 GHz microwave furnace without decomposition. Microwave sintered samples showed better densification behavior than conventional sintered samples. The higher density observed in the case of microwave sintered samples was attributed to volumetric fast heating. X-ray diffraction results of conventionally sintered samples showed β-SiAlON, tetragonal ZrO2 and ZrN phases, while, ZrO2 reacted with nitrogen and completely transformed to ZrN in the case of microwave sintered samples. The aspect ratios of microwave sintered β-SiAlON grains were higher than conventional sintered samples whereas, hardness remained lower.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.matdes.2010.02.042

Additional details

Identifiers

DOI
10.1016/j.matdes.2010.02.042;
PII
S0261-3069(10)00143-3;

Publishing Information

Journal Title
Materials and Design
Journal Volume
31
Journal Issue
8
Journal Page Range
p. 3641-3646
ISSN
0261-3069
CODEN
MADSD2

Conference

Title
International conference on materials for advanced technologies 2009
Dates
28 Jun - 3 Jul 2009
Place
Singapore (Singapore)

Optional Information

Copyright
Copyright (c) 2010 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.