Synthesis and characterization of novel 4-aminobenzoate interleaved with zinc layered hydroxide for potential sunscreen application
Creators
- 1. Sultan Idris Education University, Department of Chemistry, Faculty of Science and Mathematics (Malaysia)
- 2. Universiti Teknologi Mara, School of Chemistry and Environmental, Faculty of Applied Science (Malaysia)
Description
4-aminobenzoic acid (4-AB) interleaved with zinc layered hydroxide (ZAB) was successfully synthesized from 4-AB and zinc oxide (ZnO) by using co-precipitation method. The PXRD pattern of ZAB with a basal spacing of 23.2 Å has confirmed that 4-AB interleaved into zinc layered hydroxide (ZLH) inorganic interlayer. The interleaved compound was also verified with the presence of COO– and aromatic N–C groups observed at 1518 cm−1 and 1174 cm−1, respectively, in the FTIR spectrum. The results were supported by the presence of 18.7% carbon composition in the ZAB material obtained from TGA analysis. Morphological studies showed that ZAB material is a flake-like shape with different sizes. Further characterizations of the resulting compounds were also studied by using BET/BJH, ICP and CHNS analyses.
Additional details
Identifiers
Publishing Information
- Journal Title
- Journal of Porous Materials
- Journal Volume
- 26
- Journal Issue
- 3
- Journal Page Range
- p. 717-722
- ISSN
- 1380-2224
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 54104202
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- AROMATICS; CARBON; COPRECIPITATION; FOURIER TRANSFORM SPECTROMETERS; HYDROXIDES; INFRARED SPECTRA; POWDERS; THERMAL GRAVIMETRIC ANALYSIS; X-RAY DIFFRACTION; ZINC; ZINC OXIDES
- Descriptors DEC
- CHALCOGENIDES; CHEMICAL ANALYSIS; COHERENT SCATTERING; DIFFRACTION; ELEMENTS; GRAVIMETRIC ANALYSIS; HYDROCARBONS; HYDROGEN COMPOUNDS; MEASURING INSTRUMENTS; METALS; NONMETALS; ORGANIC COMPOUNDS; OXIDES; OXYGEN COMPOUNDS; PRECIPITATION; QUANTITATIVE CHEMICAL ANALYSIS; SCATTERING; SEPARATION PROCESSES; SPECTRA; SPECTROMETERS; THERMAL ANALYSIS; ZINC COMPOUNDS
Optional Information
- Copyright
- Copyright (c) 2019 Springer Science+Business Media, LLC, part of Springer Nature