Calibration of quantitative neutron radiography method for moisture measurement

Quantitative measurements of moisture and hydrogenous matter in building materials by neutron radiography (NR) are regularly performed at TRIGA Mark II research of 'Jozef Stefan' Institute in Ljubljana. Calibration of quantitative method is performed using standard brick samples with known moisture content and also with a secondary standard, plexiglas step wedge. In general, the contribution of scattered neutrons to the neutron image is not determined explicitly what introduces an error to the measured signal. Influence of scattered neutrons is significant in regions with high gradients of moisture concentrations, where the build up of scattered neutrons causes distortion of the moisture concentration profile. In this paper detailed analysis of validity of our calibration method for different geometrical parameters is presented. The error in the measured hydrogen concentration is evaluated by an experiment and compared with results obtained by Monte Carlo calculation with computer code MCNP 4B. Optimal conditions are determined for quantitative moisture measurements in order to minimize the error due to scattered neutrons. The method is tested on concrete samples with high moisture content.(author)