Published September 1978
| Version v1
Journal article
Chromatography of metal ions with a thioglycolate chelating resin
Description
The synthesis and properties of a chelating resin containing a thioglycoloyloxymethyl functional group are described. This resin retains silver(I), bismuth(III), tin(IV), antimony(III), mercury(II), and gold(III) from 0.1 M acid and cadmium(II), lead(II), and uranium(VI) from pH 3.5 solution. On a column containing this resin, separations of several of these metal ions are obtained by elution with acetate and hydrochloric acid eluents. Application to real samples is demonstrated by the successful analysis of NBS samples for antimony, and of acidic brine solutions for traces of mercury(II). 5 figures, 2 tables
Additional details
Publishing Information
- Journal Title
- Anal. Chem.
- Journal Volume
- 50
- Journal Issue
- 11
- Series
- Anal. Chem.
- Journal Page Range
- 1504-1508
INIS
- Country of Publication
- United States
- Country of Input or Organization
- United States
- INIS RN
- 10447754
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- ABSORPTION SPECTRA; ACCURACY; ACETATES; ANTIMONY; BISMUTH; BRINES; CADMIUM; COMPARATIVE EVALUATIONS; GOLD; HYDROCHLORIC ACID; LEACHING; LEAD; LIQUID COLUMN CHROMATOGRAPHY; MEDIUM TEMPERATURE; MERCURY; PH VALUE; QUANTITATIVE CHEMICAL ANALYSIS; RESINS; SILVER; SPECIFICATIONS; SYNTHESIS; TEMPERATURE DEPENDENCE; TIN; URANIUM
- Descriptors DEC
- ACTINIDES; CARBOXYLIC ACID SALTS; CHEMICAL ANALYSIS; CHLORINE COMPOUNDS; CHROMATOGRAPHY; DISSOLUTION; ELEMENTS; HALOGEN COMPOUNDS; HYDROGEN COMPOUNDS; INORGANIC ACIDS; METALS; ORGANIC COMPOUNDS; ORGANIC POLYMERS; POLYMERS; SEPARATION PROCESSES; SPECTRA; TRANSITION ELEMENTS