Synthesis of a mesoporous silica hollow microsphere using polyvinyl alcohol
Creators
- 1. Department of Chemistry, Anna University, Chennai - 600 025, Tamil Nadu (India)
Description
A mesoporous silica hollow microsphere was synthesized in the presence of polyvinyl alcohol for the first time. The synthesized material was characterized by various instrumental techniques such as small-angle X-ray scattering, scanning electron microscopy, transmission electron microscopy, N2 adsorption measurement and Fourier transform infrared spectroscopy. I have succeeded in incorporating an Ultraviolet ray absorber, 2, 2', 4, 4' tetrahydroxy benzophenone by mixing it after synthesis. However an attempt to incorporate by mixing before synthesizing it changes the morphology. In addition to polyvinyl alcohol, the use of other polymers such as polyvinyl pyrrolidine and polyethylene glycol also changes the morphology into dry leaves or fibers
Availability note (English)
Available from http://dx.doi.org/10.1016/j.msec.2007.11.007Additional details
Identifiers
- DOI
- 10.1016/j.msec.2007.11.007;
- PII
- S0928-4931(07)00249-4;
Publishing Information
- Journal Title
- Materials Science and Engineering. C, Biomimetic Materials, Sensors and Systems
- Journal Volume
- 28
- Journal Issue
- 8
- Journal Page Range
- p. 1260-1264
- ISSN
- 0928-4931
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 40075265
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- ADSORPTION; BENZOPHENONE; FIBERS; FOURIER TRANSFORM SPECTROMETERS; MORPHOLOGY; POLYETHYLENE GLYCOLS; PVA; SCANNING ELECTRON MICROSCOPY; SILICA; SMALL ANGLE SCATTERING; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION
- Descriptors DEC
- ALCOHOLS; COHERENT SCATTERING; DIFFRACTION; ELECTRON MICROSCOPY; GLYCOLS; HYDROXY COMPOUNDS; KETONES; MEASURING INSTRUMENTS; MICROSCOPY; MINERALS; ORGANIC COMPOUNDS; ORGANIC POLYMERS; OXIDE MINERALS; POLYMERS; POLYVINYLS; SCATTERING; SORPTION; SPECTROMETERS
Optional Information
- Copyright
- Copyright (c) 2007 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.