Microwave-assisted synthesis and characterization of nickel ferrite nanoparticles
- 1. Department of Applied Chemistry, Shri G. S. Institute of Technology and Science, Indore Madhyapradesh (India)
- 2. Department of Applied Physics, Shri G. S. Institute of Technology and Science, Indore Madhyapradesh (India)
Description
Nickel ferrite nanoparticles (NiFe2O4) were successfully prepared by microwave-assisted combustion method (MWAC) using citric Electron acid as a chelating agent. NiFe2O4 nanoparticles were characterized by X-ray diffraction (XRD) pattern, Scanning Microscopy (SEM), Fourier transform infrared (FTIR) and UV-Visible techniques. XRD analysis revealed that NiFe2O4 nanoparticles have spinel cubic structure with the average crystalline size of 26.38 nm. SEM analysis revealed random and porous structural morphology of particles and FTIR showed absorption bands related to octahedral and tetrahedral sites, in the range 400–600cm−1 which strongly favor the formation of NiFe2O4 nanoparticles. The optical band gap is determined by UV Visible method and found to be 5.4 eV
Additional details
Identifiers
- DOI
- 10.1063/1.4929187;
Publishing Information
- Journal Title
- AIP Conference Proceedings
- Journal Volume
- 1675
- Journal Issue
- 1
- Journal Page Range
- p. 020029-020029.4
- ISSN
- 0094-243X
- CODEN
- APCPCS
Conference
- Title
- 4. national conference on advanced materials and radiation physics
- Acronym
- AMRP-2015
- Dates
- 13-14 Mar 2015
- Place
- Longowal (India)
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 47058861
- Subject category
- S36: MATERIALS SCIENCE;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- ABSORPTION; ABSORPTION SPECTROSCOPY; CHELATING AGENTS; ELECTRONS; EV RANGE; FERRITES; FOURIER TRANSFORMATION; INFRARED SPECTRA; MICROWAVE RADIATION; MORPHOLOGY; NANOPARTICLES; NICKEL COMPOUNDS; POROUS MATERIALS; SCANNING ELECTRON MICROSCOPY; SPINELS; SYNTHESIS; VISIBLE SPECTRA; X-RAY DIFFRACTION
- Descriptors DEC
- COHERENT SCATTERING; DIFFRACTION; ELECTROMAGNETIC RADIATION; ELECTRON MICROSCOPY; ELEMENTARY PARTICLES; ENERGY RANGE; FERMIONS; FERRIMAGNETIC MATERIALS; INTEGRAL TRANSFORMATIONS; IRON COMPOUNDS; LEPTONS; MAGNETIC MATERIALS; MATERIALS; MICROSCOPY; MINERALS; OXIDE MINERALS; OXYGEN COMPOUNDS; PARTICLES; RADIATIONS; SCATTERING; SORPTION; SPECTRA; SPECTROSCOPY; TRANSFORMATIONS; TRANSITION ELEMENT COMPOUNDS
Optional Information
- Notes
- (c) 2015 AIP Publishing LLC