Published 1987 | Version v1
Journal article

Electrochemical oxidation of oxygen-containing Mo(6) compounds on inert electrode in chloride melts

  • 1. AN Ukrainskoj SSR, Kiev. Inst. Obshchej i Neorganicheskoj Khimii

Description

The method of current-voltage measurements in the 1-50 V/s range of polarization rates was used to study oxidation of oxygen containing Mo(6) compounds on an anode of glassy carbon in the KCl-NaCl (00 deg C) melt. Electrochemical stability of Mo(6) compounds decreases in the series MoO42->MoO3>Mo2O72-. Change in acidic main properties of (PO3-, Ca2+, F-) melt does not essentially affect the kinetics and the mechanism of the anode process. Addition of strong acids (of Al3+ type) result in decomposition of the mentioned compounds with formation of Mo oxides and oxychlorides of lower valence

Additional details

Additional titles

Original title (Russian)
Электрохимическое окисление кислородсодержащих соединений Мо(6) на инертном электроде в хлоридных расплавах

Publishing Information

Journal Title
Ukr. Khim. Zh.
Journal Volume
53
Journal Issue
12
Series
Ukr. Khim. Zh.
Journal Page Range
1286-1288
ISSN
0041-6045
CODEN
UKZHA