Published February 2019 | Version v1
Journal article

Analysis and detection of low-energy electrons in scanning electron microscopes using a Bessel box electron energy analyser

  • 1. Department of Electronic Engineering, University of York, York (United Kingdom)
  • 2. Department of Physics, University of York, York (United Kingdom)
  • 3. Department of Physics, ETH Zurich (Switzerland)
  • 4. Department of Physics, Istanbul Technical University, Istanbul (Turkey)
  • 5. York Probe Sources Ltd, York (United Kingdom)

Description

Highlights: • A new compact electron analyser and detector for use in scanning field emission microscopy is simulated, designed, constructed and characterised. • The successful acquisition of an electron spectrum showing the secondary electron peak and carbon Auger signal from a sample of graphene on copper is demonstrated. • A resolution of 0.3% has been numerically computed and experimentally verified for the analyser. - Abstract: The interpretation of images generated by scanning electron microscopes (SEMs) requires quantifiable and well-understood contrast. Furthermore, recent interest in probing samples using low-energy electrons to extract surface information is pushing towards the quantification of relative contrast in secondary-electron (SE) images. The detection and analysis of low-energy SEs remains at the heart of the development of such instruments and techniques. However, state-of-the-art SE detectors in most SEMs, which are largely using in-lens configurations, are mainly designed to favour the collection of primary-induced SEs, and hence fail to provide electron energy information that could be related to the sample composition. Here, we report on the development of a novel SE detector which makes use of the Bessel box (BB) electron energy analyser. We demonstrate a very compact analyser design (~a volume of 12 mm3) through simulations and by acquiring an electron spectrum from a sample of graphene on copper. A resolution of 0.3% has been numerically computed and experimentally verified for the BB analyser.

Availability note (English)

Available from http://dx.doi.org/10.1016/j.elspec.2019.02.002

Additional details

Identifiers

DOI
10.1016/j.elspec.2019.02.002;
PII
S0368204818301853;

Publishing Information

Journal Title
Journal of Electron Spectroscopy and Related Phenomena
Journal Issue
in press
Journal Page Range
vp.
ISSN
0368-2048
CODEN
JESRAW

INIS

Country of Publication
Netherlands
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
51051911
Subject category
S46: INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
Descriptors DEI
DESIGN; ELECTRON SPECTRA; ION MICROSCOPY; SCANNING ELECTRON MICROSCOPY
Descriptors DEC
ELECTRON MICROSCOPY; MICROSCOPY; SPECTRA

Optional Information

Notes
© 2019 Published by Elsevier B.V.