Analysis and detection of low-energy electrons in scanning electron microscopes using a Bessel box electron energy analyser
Creators
- 1. Department of Electronic Engineering, University of York, York (United Kingdom)
- 2. Department of Physics, University of York, York (United Kingdom)
- 3. Department of Physics, ETH Zurich (Switzerland)
- 4. Department of Physics, Istanbul Technical University, Istanbul (Turkey)
- 5. York Probe Sources Ltd, York (United Kingdom)
Description
Highlights: • A new compact electron analyser and detector for use in scanning field emission microscopy is simulated, designed, constructed and characterised. • The successful acquisition of an electron spectrum showing the secondary electron peak and carbon Auger signal from a sample of graphene on copper is demonstrated. • A resolution of 0.3% has been numerically computed and experimentally verified for the analyser. - Abstract: The interpretation of images generated by scanning electron microscopes (SEMs) requires quantifiable and well-understood contrast. Furthermore, recent interest in probing samples using low-energy electrons to extract surface information is pushing towards the quantification of relative contrast in secondary-electron (SE) images. The detection and analysis of low-energy SEs remains at the heart of the development of such instruments and techniques. However, state-of-the-art SE detectors in most SEMs, which are largely using in-lens configurations, are mainly designed to favour the collection of primary-induced SEs, and hence fail to provide electron energy information that could be related to the sample composition. Here, we report on the development of a novel SE detector which makes use of the Bessel box (BB) electron energy analyser. We demonstrate a very compact analyser design (~a volume of 12 mm3) through simulations and by acquiring an electron spectrum from a sample of graphene on copper. A resolution of 0.3% has been numerically computed and experimentally verified for the BB analyser.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.elspec.2019.02.002Additional details
Identifiers
- DOI
- 10.1016/j.elspec.2019.02.002;
- PII
- S0368204818301853;
Publishing Information
- Journal Title
- Journal of Electron Spectroscopy and Related Phenomena
- Journal Issue
- in press
- Journal Page Range
- vp.
- ISSN
- 0368-2048
- CODEN
- JESRAW
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 51051911
- Subject category
- S46: INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY; S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY;
- Descriptors DEI
- DESIGN; ELECTRON SPECTRA; ION MICROSCOPY; SCANNING ELECTRON MICROSCOPY
- Descriptors DEC
- ELECTRON MICROSCOPY; MICROSCOPY; SPECTRA
Optional Information
- Notes
- © 2019 Published by Elsevier B.V.