Published March 1985 | Version v1
Journal article Metadata-only

Microscale synthesis of volatile, 14C-labeled acid chlorides

Creators

  • 1. Syntex (U.S.A.) Inc., Palo Alto, CA

Description

A method for the microscale (one mmole) synthesis of volatile, 14C-labelled acid chlorides from Ba14CO3 using vacuum line techniques is described. By a judicious choice of reagents, desired intermediates and products may be isolated in high yield by simple vacuum transfer techniques without fractionation. (author)

Additional details

Publishing Information

Journal Title
J. Labelled Compd. Radiopharm.
Journal Volume
22
Journal Issue
3
Series
J. Labelled Compd. Radiopharm.
Journal Page Range
287-292
ISSN
0362-4803

INIS

Country of Publication
United Kingdom
Country of Input or Organization
United Kingdom
INIS RN
16063200
Subject category
S38: RADIATION CHEMISTRY, RADIOCHEMISTRY AND NUCLEAR CHEMISTRY;
Descriptors DEI
CARBON 14 COMPOUNDS; CHEMICAL PREPARATION; CHLORIDES; ORGANIC ACIDS; VOLATILITY
Descriptors DEC
CARBON COMPOUNDS; CHLORINE COMPOUNDS; HALIDES; HALOGEN COMPOUNDS; ORGANIC COMPOUNDS; SYNTHESIS