Published July 2007 | Version v1
Journal article

A different approach to X-ray stress analysis

  • 1. Massachusetts Institute of Technology, Room 13-5065, 77 Massachusetts Ave., Cambridge, MA (United States)

Description

A different approach to X-ray stress analysis has been developed. At the outset, it must be noted that the material to be analyzed is assumed homogeneous and isotropic. If a sphere with radius r within a specimen is subjected to a state of stress, the sphere is deformed into an ellipsoid. The semi-axes of the ellipsoid have the values of (r + εx), (r + εy), and (r + εz), which are replaced by dx, dy, and dz, or for the cubic case, ax, ay, and az. In this technique, at a particular φ angle (see ), the two-theta position of a high angle (hkl) peak is determined at ψ angles of 0, 15, 30, and 45o. These measurements are repeated for 3 to 6 φ angles in steps of 30o. The dφψ or aφψ values are then determined from the peak positions. The data is then fitted to the general quadratic equation for an ellipsoid by the method of least squares. From the coefficients of the quadratic equation, the angle between the laboratory and the specimen coordinates (direction of the principle stress) can be determined. Applying the general rotation of axes equations to the quadratic, the equation of the ellipse in the x-y plane is determined. The ax, ay, and az values for the principal axes of the lattice parameter ellipsoid are then evaluated. It is then possible to determine the unstressed a0 value from Hooke's Law using ax, ay, and az. The magnitude of the principal strains/stresses is then determined

Availability note (English)

Available from http://dx.doi.org/10.1016/j.sab.2007.03.013

Additional details

Identifiers

DOI
10.1016/j.sab.2007.03.013;
PII
S0584-8547(07)00067-5;

Publishing Information

Journal Title
Spectrochimica Acta. Part B, Atomic Spectroscopy
Journal Volume
62
Journal Issue
6-7
Journal Page Range
p. 529-532
ISSN
0584-8547
CODEN
SAASBH

Conference

Title
18. international congress on X-ray optics and microanalysis
Acronym
ICXOM 2005
Dates
25-30 Sep 2005
Place
Frascati, Rome (Italy)

INIS

Country of Publication
Netherlands
Country of Input or Organization
International Atomic Energy Agency (IAEA)
INIS RN
39081081
Subject category
S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
Resource subtype / Literary indicator
Conference
Descriptors DEI
LATTICE PARAMETERS; LEAST SQUARE FIT; STRESS ANALYSIS; X RADIATION; X-RAY DIFFRACTION
Descriptors DEC
COHERENT SCATTERING; DIFFRACTION; ELECTROMAGNETIC RADIATION; IONIZING RADIATIONS; MATHEMATICAL SOLUTIONS; MAXIMUM-LIKELIHOOD FIT; NUMERICAL SOLUTION; RADIATIONS; SCATTERING

Optional Information

Copyright
Copyright (c) 2007 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.