Growth and characterization of two-dimensional nanostructures
Description
Two dimensional nanostructures of palladium, nickel, silver and gadolinium were grown by means of physical evaporation in atmospheres of high vacuum and ultra high vacuum. The qualitative characterization, in situ, of the nanostructures was carried out with techniques of surface analysis: Auger electron spectroscopy and X-ray photoelectron spectroscopy (XPS). The model for the quantification of contaminants in the nanostructures, was proposed by Seah and Shirley, and was made using the spectra XPS measured in situ in the atmospheres of vacuum. For the two-dimensional nanostructures of gadolinium of thicknesses 8 Å, 16 Å, 24 Å, 32 Å, 36 Å, 44 Å, 50 Å, 61 Å, 77 Å, 81 Å, 92 Å and 101 Å, were obtained optical spectra of transmission measured in situ. An band of absorption centered at approximately 2,40 eV is obtained by an increase in the dynamic conductivity from the optical constants, i.e. refractive index and extinction coefficient, of the nanostructure of gadolinium. In addition, the optical constants for the gadolinium nanostructures have presented a maximum of 80 Å of thickness and then it was continued a decreasing tendency toward the values that were reported in the literature for bulk of gadolinium. (author)
Availability note (English)
Available from Biblioteca Luis Demetrio Tinoco, Universidad de Costa RicaAbstract (Spanish)
Nanoestructuras bidimensionales de paladio, niquel, plata y gadolinio fueron crecidas por medio de evaporacion fisica en atmosferas de alto vacio y ultra alto vacio. La caracterizacion cualitativa, in situ, de las nanoestructuras fue llevada a cabo con las tecnicas de analisis de superficies: espectroscopia de electrones Auger (AES) y espectroscopia de fotoelectrones de rayos X (XPS). El modelo para la cuantificacion de los contaminantes presentes en las nanoestructuras, fue propuesto por Seah y Shirley, y fue hecho utilizando los espectros XPS medidos in situ en las atmosferas de vacio. Para las nanoestructuras bidimensionales de gadolinio de espesores 8 Å, 16 Å, 24 Å, 32 Å, 36 Å, 44 Å, 50 Å, 61 Å, 77 Å, 81 Å, 92 Å y 101 Å, se han obtenido espectros opticos de transmision medidos in situ. Una banda de absorcion centrada en aproximadamente 2,40 eV es obtenida por un incremento en la conductividad dinamica a partir de las constantes opticas, i.e. indice de refraccion y coeficiente de extincion, de la nanoestructura de gadolinio. Ademas, las constantes opticas para las nanoestructuras de gadolinio han presentado un maximo de 80 Å de espesor y despues ha continuado una tendencia decreciente hacia los valores que fueron reportados en la literatura para el bulk de gadolinio. (autor)Additional details
Additional titles
- Original title (Spanish)
- Crecimiento y caracterizacion de nanoestructuras bidimensionales
Publishing Information
- Imprint Place
- San Jose (Costa Rica)
- Imprint Pagination
- 166 p.
INIS
- Country of Publication
- Costa Rica
- Country of Input or Organization
- Costa Rica
- INIS RN
- 45013656
- Subject category
- S36: MATERIALS SCIENCE; S75: CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY; S77: NANOSCIENCE AND NANOTECHNOLOGY;
- Resource subtype / Literary indicator
- Numerical Data, Thesis, Non-conventional Literature
- Descriptors DEI
- AUGER ELECTRON SPECTROSCOPY; CONTROLLED ATMOSPHERES; EXPERIMENTAL DATA; GADOLINIUM; NANOSTRUCTURES; NICKEL; ON-SITE INSPECTION; OPTICAL PROPERTIES; PALLADIUM; PRESSURE RANGE MICRO PA; SILVER; VACUUM EVAPORATION; VACUUM SYSTEMS; X-RAY PHOTOELECTRON SPECTROSCOPY
- Descriptors DEC
- ATMOSPHERES; DATA; ELECTRON SPECTROSCOPY; ELEMENTS; EVAPORATION; INFORMATION; INSPECTION; METALS; NUMERICAL DATA; PHASE TRANSFORMATIONS; PHOTOELECTRON SPECTROSCOPY; PHYSICAL PROPERTIES; PLATINUM METALS; PRESSURE RANGE; RARE EARTHS; SPECTROSCOPY; TRANSITION ELEMENTS
Optional Information
- Notes
- Figs., tabs., refs.