Separating the influence of electric charges in magnetic force microscopy images of inhomogeneous metal samples
Creators
- 1. Laboratory of Nondestructive Testing, Corrosion and Welding, Rio de Janeiro, RJ 21941-596 (Brazil)
- 2. Department of Metallurgical and Materials Engineering – UFRJ, Rio de Janeiro, RJ 21941-972 (Brazil)
- 3. São Paulo State University – UNESP, Sorocaba, SP 18087-180 (Brazil)
- 4. Brazilian Nanotechnology National Laboratory, Campinas, SP 18083-970 (Brazil)
- 5. Petrobras, Rio de Janeiro, RJ 21040-000 (Brazil)
- 6. Gleb Wataghin Institute of Physics, University of Campinas, SP 13083859 (Brazil)
Description
Highlights: • Magnetic and electrical signals have been distinguished using MFM and EFM techniques. • MFM images need to be interpreted with care due to the influence of electrical charges. • Magnetic contribution is separated from the electrical contribution using an external magnet. In this study, we investigate artifacts arising from electric charges present in magnetic force microscopy images. Therefore, we use two austenitic steel samples with different microstructural conditions. Furthermore, we examine the influence of the surface preparation, like etching, in magnetic force images. Using Kelvin probe force microscopy we can quantify the charges present on the surface. Our results show that electrical charges give rise to a signature in the magnetic force microscopy, which is indistinguishable from a magnetic signal. Our results on two differently aged steel samples demonstrate that the magnetic force microscopy images need to be interpreted with care and must be corrected due to the influence of electrical charges present. We discuss three approaches, how to identify these artifacts – parallel acquisition of magnetic force and electric force images on the same position, sample surface preparation to decrease the presence of charges and inversion of the magnetic polarization in two succeeding measurement.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.jmmm.2017.09.041Additional details
Identifiers
- DOI
- 10.1016/j.jmmm.2017.09.041;
- PII
- S0304885317320231;
Publishing Information
- Journal Title
- Journal of Magnetism and Magnetic Materials
- Journal Volume
- 446
- Journal Page Range
- p. 239-244
- ISSN
- 0304-8853
- CODEN
- JMMMDC
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 53014593
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- AGING; ATOMIC FORCE MICROSCOPY; AUSTENITIC STEELS; CARBIDES; ELECTRIC CHARGES; ETCHING; IMAGES; MAGNETIC FIELDS; MAGNETIC PROPERTIES; MAGNETS; METALS; MICROSTRUCTURE; POLARIZATION; SIGNALS
- Descriptors DEC
- ALLOYS; CARBON ADDITIONS; CARBON COMPOUNDS; ELEMENTS; EQUIPMENT; IRON ALLOYS; IRON BASE ALLOYS; MICROSCOPY; PHYSICAL PROPERTIES; STEELS; SURFACE FINISHING; TRANSITION ELEMENT ALLOYS
Optional Information
- Copyright
- Copyright (c) 2017 Elsevier B.V. All rights reserved.