Published 1980
| Version v1
Journal article
Evaluation of treatments to attain isotopic equilibration of plutonium preceding the resin bead technique for mass spectrometric assay analysis of spent reactor fuel
Description
Ten chemical treatments are evaluated for the attainment of isotopic equilibration of plutonium prior to its sorption on resin beads for assay of dissolved reactor fuel by isotope-dilution mass spectrometry. The one consistently reliable treatment is reduction to Pu(III) with heated ferrous sulfamate followed by oxidation to Pu(IV) with heated sodium nitrite
Additional details
Publishing Information
- Journal Title
- Anal. Lett.
- Journal Volume
- 13
- Journal Issue
- A17
- Series
- Anal. Lett.
- Journal Page Range
- 1487-1495
- ISSN
- 0003-2719
INIS
- Country of Publication
- United States
- Country of Input or Organization
- United States
- INIS RN
- 12606687
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; S98: NUCLEAR DISARMAMENT, SAFEGUARDS AND PHYSICAL PROTECTION;
- Descriptors DEI
- ADSORPTION; EQUILIBRIUM; IRON COMPOUNDS; ISOTOPE DILUTION; ISOTOPE RATIO; MASS SPECTROSCOPY; NITRITES; OXIDATION; PLUTONIUM; REDUCTION; RESINS; SAFEGUARDS; SODIUM COMPOUNDS; SPENT FUELS; SULFONIC ACIDS; URANIUM
- Descriptors DEC
- ACTINIDES; ALKALI METAL COMPOUNDS; CHEMICAL REACTIONS; ELEMENTS; ENERGY SOURCES; FUELS; ISOTOPE APPLICATIONS; METALS; NITROGEN COMPOUNDS; NUCLEAR FUELS; ORGANIC ACIDS; ORGANIC COMPOUNDS; ORGANIC POLYMERS; ORGANIC SULFUR COMPOUNDS; OXYGEN COMPOUNDS; POLYMERS; REACTOR MATERIALS; SPECTROSCOPY; TRACER TECHNIQUES; TRANSITION ELEMENT COMPOUNDS; TRANSURANIUM ELEMENTS