Procedure for the preparation of stabilized ZrO2 mixed oxide powders with high sinterability
Description
The invention is directed at a procedure for the preparation of stabilized mixed oxide powders (e.g. with CaO, MgO, Y2O3) with high sinterability for the production of solid electrolyte ceramics. These ceramics are also applied to power plant instrumentation. The procedure leads to a stabilized ZrO2 mixed oxide of highest homogeneity without additional homogeneization steps. The two compounds are precipitated in an optimed homogeneous distribution in such a way that a carbonato-zirconate complex solution is produced by dissolving the zirconium compound in an excess of alkali or ammonium carbonate. A separately prepared solution mixture consisting of an acid and a stabilizer salt is added. The precipitated basic Zr-carbonate with its homogeneous distribution of stabilizer cations is calcined to ZrO2 mixed oxide powder
Availability note (English)
MF available from INIS under the Report Number.Files
18093997.pdf
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Additional details
Additional titles
- Original title (German)
- Verfahren zur Herstellung eines stabilisierten ZrO
Publishing Information
- Imprint Pagination
- 3 p.
- IPC:
- Int. Cl. C01g 25/02.
- IPC
- Int. Cl. C01g 25/02.
- Patent number
- DD patent document 239396/A/
INIS
- Country of Publication
- German Democratic Republic
- Country of Input or Organization
- German Democratic Republic
- INIS RN
- 18093997
- Subject category
- S36: MATERIALS SCIENCE;
- Descriptors DEI
- CALCINATION; CARBONATES; CERAMICS; CHEMICAL PREPARATION; POWDERS; SINTERING; SPECIFICATIONS; ZIRCONATES; ZIRCONIUM COMPLEXES; ZIRCONIUM OXIDES
- Descriptors DEC
- CARBON COMPOUNDS; CHALCOGENIDES; CHEMICAL REACTIONS; COMPLEXES; DECOMPOSITION; FABRICATION; OXIDES; OXYGEN COMPOUNDS; PYROLYSIS; SYNTHESIS; TRANSITION ELEMENT COMPLEXES; TRANSITION ELEMENT COMPOUNDS; ZIRCONIUM COMPOUNDS