Published January 2019 | Version v1
Journal article

Trifluoroacetylation of N-Substituted 1H-1,2-Diazaphenalenes of the Naphthalene and Acenaphthene Series

  • 1. Southern Federal University, Research Institute of Physical and Organic Chemistry (Russian Federation)
  • 2. Russian Academy of Sciences, Kurnakov Institute of General and Inorganic Chemistry (Russian Federation)

Description

The acylation of N-substituted 3-methyl-1H-1,2-diazaphenalenes of the naphthalene and acenaphthene series with trifluoroacetic anhydride gave mono- and diacylated products. Despite the presence of a bulky substituent on the pyrrole type nitrogen atom, the trifluoroacetyl group entered the peri position with respect to that substituent. The product structure was confirmed by X-ray analysis.

Additional details

Identifiers

Publishing Information

Journal Title
Russian Journal of Organic Chemistry
Journal Volume
55
Journal Issue
1
Journal Page Range
p. 87-92
ISSN
1070-4280

Optional Information

Copyright
Copyright (c) 2019 Pleiades Publishing, Ltd.