Published April 15, 1983 | Version v1
Journal article

Development of a new energy scanned (4-20 keV) EXAFS-II spectrometer at LURE

  • 1. Paris-6 Univ., 75 (France). Physique des Liquides et Electrochimie
  • 2. Nancy-1 Univ., 54 (France). Interactions Moleculaires
  • 3. Laboratoire pour l'Utilisation du Rayonnement Electromagnetique (LURE), Paris-11 Univ., 91 - Orsay (France)

Description

The new energy scanned EXAFS spectrometer (EXAFS-II) which has been recently installed on beam line D2 at LURE (Orsay) is described in this paper. The key component of the spectrometer is a versatile monochromator operating in a vacuum of approx.=10-3 Torr. It uses a vertically dispersing two separated crystal design in the (+, -) arrangement which offers an exit beam of constant offset and direction relative to the incident beam, optional sagittal focusing and order sorting. Also optional is the energy modulation provided by a piezoelectric transducer capable of small angular oscillations of up to 1 kHz. Conventional gas filled ion chambers are used as detectors - even for fluorescence EXAFS - but each detector is incorporating a home-made, ultralow noise, fast preamplifier capable of detecting weak signals even at a high modulation frequency (1 kHz). Glitch-free spectra have been recorded over the whole energy range covered by DCI in standard operating conditions. (orig.)

Additional details

Publishing Information

Journal Title
Nucl. Instrum. Methods Phys. Res.
Journal Volume
208
Journal Issue
1-3
Series
Nucl. Instrum. Methods Phys. Res.
Journal Page Range
625-630
ISSN
0029-554X

Conference

Title
International conference on X-Ray and VUV synchrotron radiation instrumentation.
Dates
9-13 Aug 1982.
Place
Hamburg (Germany, F.R.).