Crystal Structure of Pyrographite and Catalytically Deposited Carbon

By the method of X-ray structure analysis were investigated the crystal structure and phase content of catalytically deposited on the metal nickel from the gas phase (600 degree C and 800 degree C) carbon and pyrographite produced by high temperature treatment (3000...3070 degree C, 30 minutes) of the carbon material of the SP 'Uglecomposit'. Pyrographite has high rate of crystal structure perfection, parameters of the area of the coherent scattering that are close to the Ceylon graphite; d002 equal to (3,361±0,005) A, graphitizing rate - 1; dimensions of the crystal grating: Lc not less 5000 A, La - (380±50) A. Pyrographite grains are mostly oriented in perpendicular to the deposition plane. Catalytically deposited carbon consists of the graphite phase, amorphous carbon and metallic nickel. Graphite phase has a middle rate of crystal structure perfection: d002=(3,3986±0,0005) A, graphitizing rate - 0,48, area of the coherent scattering: Lc=140...180 A, La=100...150 A. The amorphous carbon content is up to 30...42 % from the carbon phases mass