Hydrothermal synthesis of nanostructured zinc oxide and study of their optical properties
Creators
- 1. Laboratoire de Chimie de la Matière Condensée IPEIT, Université de Tunis, 2 rue Jawaher Lel Nehru 1008, B.P. 229 Montfleury, Tunis (Tunisia)
- 2. Faculté des Sciences de Tunis, Université Tunis El Manar, 2092 El Manar, Tunis (Tunisia)
Description
Highlights: ► Nanostructured ZnO were successfully obtained by a hydrothermal route. ► Inorganic precursor and molar ratio are key factors for morphology and particle size. ► Optical properties were also studied. -- Abstract: Nanostructured ZnO (nanorods, nanoshuttles) have been synthesized by hydrothermal approach using ZnCl2 or Zn(NO3)2·6H2O as zinc sources and cetyltrimethylammonium bromide as structure-directing agent. Techniques X-ray powder diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), UV–visible absorption, Fourier transform infrared spectroscopy (FTIR) and Raman spectroscopy have been used to characterize the structure, morphology and composition of the nanostructured zinc oxide. The optical properties of the as-obtained materials were also studied and showing that it is possible to apply the ZnO nanoshuttles and nanorods on the UV filter, photocatalysis, and special optical devices.
Availability note (English)
Available from http://dx.doi.org/10.1016/j.materresbull.2011.12.027Additional details
Identifiers
- DOI
- 10.1016/j.materresbull.2011.12.027;
- PII
- S0025-5408(11)00635-0;
Publishing Information
- Journal Title
- Materials Research Bulletin
- Journal Volume
- 47
- Journal Issue
- 3
- Journal Page Range
- p. 667-671
- ISSN
- 0025-5408
- CODEN
- MRBUAC
INIS
- Country of Publication
- United States
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 45033410
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; S36: MATERIALS SCIENCE; S77: NANOSCIENCE AND NANOTECHNOLOGY;
- Descriptors DEI
- ABSORPTION; FOURIER TRANSFORM SPECTROMETERS; FOURIER TRANSFORMATION; HYDROTHERMAL SYNTHESIS; INFRARED SPECTRA; INORGANIC COMPOUNDS; NANOSTRUCTURES; OPTICAL PROPERTIES; PARTICLE SIZE; RAMAN SPECTROSCOPY; SCANNING ELECTRON MICROSCOPY; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION; ZINC; ZINC CHLORIDES; ZINC OXIDES
- Descriptors DEC
- CHALCOGENIDES; CHLORIDES; CHLORINE COMPOUNDS; COHERENT SCATTERING; DIFFRACTION; ELECTRON MICROSCOPY; ELEMENTS; HALIDES; HALOGEN COMPOUNDS; INTEGRAL TRANSFORMATIONS; LASER SPECTROSCOPY; MEASURING INSTRUMENTS; METALS; MICROSCOPY; OXIDES; OXYGEN COMPOUNDS; PHYSICAL PROPERTIES; SCATTERING; SIZE; SORPTION; SPECTRA; SPECTROMETERS; SPECTROSCOPY; SYNTHESIS; TRANSFORMATIONS; ZINC COMPOUNDS; ZINC HALIDES
Optional Information
- Copyright
- Copyright (c) 2011 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.