Published 2017 | Version v1
Journal article

Wide-angle diamond cell for neutron scattering

Description

Here, a new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the Oak Ridge National Laboratory. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax®) pressure anvils are used. We predict a routine pressure regime up to 20 GPa with sample volumes of ~0.5 mm3. Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.

Availability note (English)

Available from https://www.osti.gov/servlets/purl/1465058; https://www.osti.gov/biblio/1465058; DOE Accepted Manuscript full text, or the publishers Best Available Version will be available free of charge after the embargo period

Additional details

Publishing Information

Journal Title
High Pressure Research
Journal Volume
37
Journal Issue
4
Journal Page Range
p. 495-506
ISSN
0895-7959

Optional Information

Contract/Grant/Project number
AC05-00OR22725
Funding organization
USDOE Office of Science - SC, Basic Energy Sciences (BES) (SC-22) (United States)
Secondary number(s)
OSTIID--1465058