Published 2010 | Version v1
Journal article

Optimal conditions for specifying formaldehyde using several reagents with the help of visible spectrometric technique

  • 1. Tishreen Univ. Faculty of Sciences, Lattakia (Syrian Arab Republic), Dept. of Chemistry

Description

This study deals with the comparison of (Acetyl acetone, Acetoacetanilide, chromotropic acid disodium salt) used as reagents for determine formaldehyde, and to fixed the optimal analytical conditions of the above signed reagents using VIS-Spectrophotometer. The optimal analytical conditions of each reagent are compared with each other in order to determine the optimal reagent and conditions which allow to determining formaldehyde as possible at its lowest detection limit. The results of this study are compared with other studies used the same reagents, but by contrast analytical conditions. The lowest detection limit for chromotropic acid disodium salt ranged between (0.0100 - 0.0125 ppm) with recovery ranged between (108.543- 119.444%) depending on the reproducibility of three sequence separated experiments (independent samples). This detection limit is twice times lower than the detection limit 0.02 ppm registered according to the study achieved by method (NIOSH 3500).(author)

Additional details

Publishing Information

Journal Title
Tishreen University Journal for Research and Scientific Studies. Basic Sciences Series
Journal Volume
32
Journal Issue
1
Journal Page Range
p. 157-171
ISSN
2079-3057

Optional Information

Notes
15 Refs., 11 Figs., 4 Tabs.