Optimal conditions for specifying formaldehyde using several reagents with the help of visible spectrometric technique
Creators
- 1. Tishreen Univ. Faculty of Sciences, Lattakia (Syrian Arab Republic), Dept. of Chemistry
Description
This study deals with the comparison of (Acetyl acetone, Acetoacetanilide, chromotropic acid disodium salt) used as reagents for determine formaldehyde, and to fixed the optimal analytical conditions of the above signed reagents using VIS-Spectrophotometer. The optimal analytical conditions of each reagent are compared with each other in order to determine the optimal reagent and conditions which allow to determining formaldehyde as possible at its lowest detection limit. The results of this study are compared with other studies used the same reagents, but by contrast analytical conditions. The lowest detection limit for chromotropic acid disodium salt ranged between (0.0100 - 0.0125 ppm) with recovery ranged between (108.543- 119.444%) depending on the reproducibility of three sequence separated experiments (independent samples). This detection limit is twice times lower than the detection limit 0.02 ppm registered according to the study achieved by method (NIOSH 3500).(author)
Additional details
Publishing Information
- Journal Title
- Tishreen University Journal for Research and Scientific Studies. Basic Sciences Series
- Journal Volume
- 32
- Journal Issue
- 1
- Journal Page Range
- p. 157-171
- ISSN
- 2079-3057
INIS
- Country of Publication
- Syrian Arab Republic
- Country of Input or Organization
- Syrian Arab Republic
- INIS RN
- 43128682
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Numerical Data
- Descriptors DEI
- ACETOACETATES; ACETYLACETONE; ANALYTICAL SOLUTION; CHROMOTROPIC ACID; COMPARATIVE EVALUATIONS; EXPERIMENTAL DATA; FORMALDEHYDE; SALTS; VISIBLE SPECTRA
- Descriptors DEC
- ALDEHYDES; CARBOXYLIC ACID SALTS; CHELATING AGENTS; DATA; EVALUATION; HYDROXY COMPOUNDS; INFORMATION; KETONES; MATHEMATICAL SOLUTIONS; NUMERICAL DATA; ORGANIC ACIDS; ORGANIC COMPOUNDS; ORGANIC SULFUR COMPOUNDS; REAGENTS; SPECTRA; SULFONIC ACIDS
Optional Information
- Notes
- 15 Refs., 11 Figs., 4 Tabs.