Published November 2009 | Version v1
Journal article

Recognition of perrhenate and pertechnetate by a neutral macrocyclic receptor

  • 1. M.V. Lomonosov Moscow State University, Moscow (Russian Federation). Department of Chemistry
  • 2. Russian Academy of Sciences, Moscow (Russian Federation). A.N. Nesmeyanov Institute of Organoelement Compounds
  • 3. New Mexico Highlands University, Las Vegas, NM (United States). Department of Natural Sciences
  • 4. Baku State University, Baku (Azerbaijan)
  • 5. Russian Academy of Sciences, Moscow (Russian Federation). A.N. Frumkin Institute of Physical Chemistry and Electrochemistry

Description

The synthesis and anion binding properties of a neutral macrocyclic receptor bearing H-bond donor coordination sites are described. The anion binding studies by use of UV-vis and 99Tc NMR methods revealed that the receptor can coordinate perrhenate and pertechnetate in dimethylsulfoxide and chloroform solutions with the relatively high binding constants, viz. log Ka > 4. The coordination mode of the perrhenate to the receptor was determined by a single-crystal X-ray diffraction analysis. (author)

Additional details

Publishing Information

Journal Title
Journal of Radioanalytical and Nuclear Chemistry
Journal Volume
282
Journal Issue
2
Journal Page Range
p. 385-389
ISSN
0236-5731
CODEN
JRNCDM

Conference

Title
Methods and applications of radioanalytical chemistry. Part 2
Acronym
MARC VIII
Dates
5-10 Apr 2009
Place
Hawaii (United States)

Optional Information

Notes
26 refs.