Published October 1991
| Version v1
Journal article
Gas chromatographic determination of tributyl phosphate, dibutyl phosphate and butyl phosphate in kerosene solutions
Description
A gas chromatographic procedure has been developed for the determination of tributyl phosphate (TBP), dibutyl phosphate (HDBP) and butyl phosphate (H2MBP) in kerosene solutions. The last two compounds were converted into their methyl esters by reaction with a solution of diazomethane in diisopropyl ether prior to analysis. The same procedure was applied to the determination of HBDP and H2MBP produced from gamma irradiation of the 30% TBP-kerosene-3 mol dm-3 HNO3 system. (author)
Additional details
Publishing Information
- Journal Title
- Analyst
- Journal Volume
- 116
- Journal Issue
- 10
- Series
- Analyst.
- Journal Page Range
- 1067-1069
- ISSN
- 0003-2654
- CODEN
- ANALA
INIS
- Country of Publication
- United Kingdom
- Country of Input or Organization
- United Kingdom
- INIS RN
- 23014081
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Descriptors DEI
- DBP; GAS CHROMATOGRAPHY; MBP; METHYLATION; TBP
- Descriptors DEC
- BUTYL PHOSPHATES; CHEMICAL REACTIONS; CHROMATOGRAPHY; ESTERS; ORGANIC COMPOUNDS; ORGANIC PHOSPHORUS COMPOUNDS; PHOSPHORIC ACID ESTERS; SEPARATION PROCESSES