The upgraded external-beam PIXE/PIGE set-up at LABEC for very fast measurements on aerosol samples
Description
At the 3 MV Tandetron accelerator of the LABEC laboratory of INFN in Florence, an external beam facility is fully dedicated to measurements of elemental composition of atmospheric aerosol. The experimental set-up hitherto used for this kind of applications has been upgraded with the replacement of a traditional Si(Li) detector for the detection of medium–high Z elements with a silicon drift detector (SDD) with a big active area (80 mm2) and 450 μm thickness, with the aim of obtaining better minimum detection limits (MDL) and reduce measuring times. The Upilex extraction window has been replaced by a more resistant one (Si3N4). A comparison between the old Si(Li) and the new SDD for aerosol samples collected on different substrata like Teflon, Kapton and Nuclepore evidenced the better performances of the SDD. It allows obtaining better results (higher counting statistics, lower MDLs) even in shorter measuring times, thus allowing very fast analysis of both daily and hourly samples
Availability note (English)
Available from http://dx.doi.org/10.1016/j.nimb.2013.05.099Additional details
Identifiers
- DOI
- 10.1016/j.nimb.2013.05.099;
- PII
- S0168-583X(13)00777-5;
Publishing Information
- Journal Title
- Nuclear Instruments and Methods in Physics Research. Section B, Beam Interactions with Materials and Atoms
- Journal Volume
- 318
- Journal Issue
- Part A
- Journal Page Range
- p. 55-59
- ISSN
- 0168-583X
- CODEN
- NIMBEU
Conference
- Title
- 13. international conference on particle induced X-ray emission
- Acronym
- PIXE 2013
- Dates
- 3-8 Mar 2013
- Place
- Gramado (Brazil)
INIS
- Country of Publication
- Netherlands
- Country of Input or Organization
- International Atomic Energy Agency (IAEA)
- INIS RN
- 45070658
- Subject category
- S46: INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- ACCELERATORS; AEROSOLS; BEAMS; COMPARATIVE EVALUATIONS; EXTRACTION; LI-DRIFTED SI DETECTORS; PERFORMANCE; PIXE ANALYSIS; SENSITIVITY; SILICON; SILICON NITRIDES; TEFLON; THICKNESS
- Descriptors DEC
- CHEMICAL ANALYSIS; COLLOIDS; DIMENSIONS; DISPERSIONS; ELEMENTS; EVALUATION; FLUORINATED ALIPHATIC HYDROCARBONS; HALOGENATED ALIPHATIC HYDROCARBONS; LI-DRIFTED DETECTORS; MATERIALS; MEASURING INSTRUMENTS; NITRIDES; NITROGEN COMPOUNDS; NONDESTRUCTIVE ANALYSIS; ORGANIC COMPOUNDS; ORGANIC FLUORINE COMPOUNDS; ORGANIC HALOGEN COMPOUNDS; ORGANIC POLYMERS; PETROCHEMICALS; PETROLEUM PRODUCTS; PLASTICS; PNICTIDES; POLYETHYLENES; POLYMERS; POLYOLEFINS; POLYTETRAFLUOROETHYLENE; RADIATION DETECTORS; SEMICONDUCTOR DETECTORS; SEMIMETALS; SEPARATION PROCESSES; SI SEMICONDUCTOR DETECTORS; SILICON COMPOUNDS; SOLS; SYNTHETIC MATERIALS; X-RAY EMISSION ANALYSIS
Optional Information
- Copyright
- Copyright (c) 2013 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.