Published February 2008
| Version v1
Book
Specification check of zircaloy using differential pulse anodic stripping voltammetry (DP-ASV): analysis of lead
Creators
- 1. Radioanalytical Chemistry Section, Bhabha Atomic Research Centre, Mumbai (India)
- 2. Radiochemistry and Isotope Group, Bhabha Atomic Research Centre, Mumbai (India)
Description
The present study demonstrates a simple, rapid and sensitive Differential Pulse Anodic Stripping Voltammetric (DP-ASV) procedure for the determination of lead at nano-gram levels in zircaloy-2 samples after successfully masking zirconium by ammonium citrate buffer. An online software programme is used for the accurate determination of peak currents. Lead concentration is calculated using standard addition technique. Preliminary results of lead are within ± 6% at ppb level in 0.25 M ammonium citrate of pH 2.5
Additional details
Publishing Information
- Publisher
- Indian Society for Electroanalytical Chemistry
- Imprint Place
- Mumbai (India)
- ISBN
- 978-81-901950-1-0
- Imprint Title
- Discussion meet on electroanalytical techniques and their applications
- Imprint Pagination
- 328 p.
- Journal Page Range
- p. 175-178
Conference
- Title
- discussion meet on electroanalytical techniques and their applications
- Acronym
- DM-ELANTE 2008
- Dates
- 25-28 Feb 2008
- Place
- Munnar (India)
INIS
- Country of Publication
- India
- Country of Input or Organization
- India
- INIS RN
- 39083028
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Conference
- Descriptors DEI
- LEAD; PH VALUE; STRIPPING; TRACE AMOUNTS; VOLTAMETRY; ZIRCALOY 2
- Descriptors DEC
- ALLOY-ZR98SN-2; ALLOYS; CHROMIUM ADDITIONS; CHROMIUM ALLOYS; CORROSION RESISTANT ALLOYS; DIRECT REACTIONS; ELEMENTS; HEAT RESISTANT MATERIALS; HEAT RESISTING ALLOYS; IRON ADDITIONS; IRON ALLOYS; MATERIALS; METALS; NICKEL ADDITIONS; NICKEL ALLOYS; NUCLEAR REACTIONS; TIN ALLOYS; TRANSFER REACTIONS; TRANSITION ELEMENT ALLOYS; ZIRCALOY; ZIRCONIUM ALLOYS; ZIRCONIUM BASE ALLOYS
Optional Information
- Notes
- 3 refs., 2 figs., 1 tab.