Published 2010 | Version v1
Journal article

Suppression of phase anomalies and side-bands on 13C NMR spectra obtained with the steady state free precession sequence

  • 1. Universidade de Sao Paulo (USP), Sao Carlos, SP (Brazil). Inst. de Quimica
  • 2. Universidade de Sao Paulo (USP), Sao Carlos, SP (Brazil). Inst. de Fisica
  • 3. EMBRAPA Instrumentacao Agropecuaria, Sao Carlos, SP (Brazil)

Description

The Steady-State Free Precession (SSFP) sequence has been widely used in low-field and low-resolution imaging NMR experiments to increase the signal-to-noise ratio (s/n) of the signals. Here, we analyzed the Scrambled Steady State - SSS and Unscrambled Steady State - USS sequences to suppress phase anomalies and sidebands of the 13C NMR spectrum acquired in the SSFP regime. The results showed that the application of the USS sequence allowed a uniform distribution of the time interval between pulses (Tp), in the established time range, allowing a greater suppression of phase anomalies and sidebands, when compared with the SSS sequence. (author)

Availability note (English)

Available from http://www.scielo.br/pdf/qn/v33n4/34.pdf

Additional details

Additional titles

Original title (Portuguese)
Supressao das anomalias de fase e batimentos laterais em espectros de RMN

Publishing Information

Journal Title
Quimica Nova On-Line
Journal Volume
33
Journal Issue
4
Journal Page Range
p. 954-956
ISSN
1678-7064