Published 2010
| Version v1
Journal article
Suppression of phase anomalies and side-bands on 13C NMR spectra obtained with the steady state free precession sequence
- 1. Universidade de Sao Paulo (USP), Sao Carlos, SP (Brazil). Inst. de Quimica
- 2. Universidade de Sao Paulo (USP), Sao Carlos, SP (Brazil). Inst. de Fisica
- 3. EMBRAPA Instrumentacao Agropecuaria, Sao Carlos, SP (Brazil)
Description
The Steady-State Free Precession (SSFP) sequence has been widely used in low-field and low-resolution imaging NMR experiments to increase the signal-to-noise ratio (s/n) of the signals. Here, we analyzed the Scrambled Steady State - SSS and Unscrambled Steady State - USS sequences to suppress phase anomalies and sidebands of the 13C NMR spectrum acquired in the SSFP regime. The results showed that the application of the USS sequence allowed a uniform distribution of the time interval between pulses (Tp), in the established time range, allowing a greater suppression of phase anomalies and sidebands, when compared with the SSS sequence. (author)
Availability note (English)
Available from http://www.scielo.br/pdf/qn/v33n4/34.pdfAdditional details
Additional titles
- Original title (Portuguese)
- Supressao das anomalias de fase e batimentos laterais em espectros de RMN
Identifiers
Publishing Information
- Journal Title
- Quimica Nova On-Line
- Journal Volume
- 33
- Journal Issue
- 4
- Journal Page Range
- p. 954-956
- ISSN
- 1678-7064
INIS
- Country of Publication
- Brazil
- Country of Input or Organization
- Brazil
- INIS RN
- 41081724
- Subject category
- S37: INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY;
- Resource subtype / Literary indicator
- Numerical Data
- Descriptors DEI
- ACETATES; CARBON 13; CHLOROFORM; EXPERIMENTAL DATA; METHYL RADICALS; NMR SPECTRA; RELAXATION TIME; SILANES; STEADY-STATE CONDITIONS
- Descriptors DEC
- ALKYL RADICALS; CARBON ISOTOPES; CARBOXYLIC ACID SALTS; CHLORINATED ALIPHATIC HYDROCARBONS; DATA; EVEN-ODD NUCLEI; HALOGENATED ALIPHATIC HYDROCARBONS; HYDRIDES; HYDROGEN COMPOUNDS; INFORMATION; ISOTOPES; LIGHT NUCLEI; NUCLEI; NUMERICAL DATA; ORGANIC CHLORINE COMPOUNDS; ORGANIC COMPOUNDS; ORGANIC HALOGEN COMPOUNDS; ORGANIC SILICON COMPOUNDS; RADICALS; SILICON COMPOUNDS; SPECTRA; STABLE ISOTOPES