Published January 1967 | Version v1
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Study of the behaviour of some heavy elements in solvents containing hydrogen fluoride

  • 1. Commissariat a l'Energie Atomique, Fontenay-aux-Roses (France). Centre d'Etudes Nucleaires

Description

The anhydrous liquid mixtures: dinitrogen tetroxide-hydrogen fluoride and antimony pentafluoride-hydrogen fluoride were studied as solvents for heavy elements interesting nuclear energy: uranium, thorium, zirconium and for some of their compounds. For N2O4-HF mixtures, electric conductivity measurements and liquid phase infrared spectra were also obtained. Uranium and zirconium tetrafluoride are much more soluble in N2O4-HF mixtures than in pure hydrogen fluoride. Uranium dissolved in these mixtures is pentavalent. In SbF5-HF mixtures, uranium dissolves with hydrogen evolution and becomes trivalent. The solid compound resulting from the dissolution is a fluoro-antimonate: U(SbF6)3. (author)

Availability note (English)

Available from INIS in electronic form

Abstract (French)

On a etudie les melanges liquides anhydres: peroxyde d'azote-acide fluorhydrique et pentafluorure d'antimoine-acide fluorhydrique comme solvants d'elements lourds interessant l'energie nucleaire: uranium, thorium, zirconium et de quelques uns de leurs composes. Pour les melanges N2O4-HF on a egalement effectue des mesures de conductivite electrique, ainsi que des spectres d'absorption infrarouge en phase liquide. Le tetrafluorure d'uranium et le tetrafluorure de zirconium sont beaucoup plus solubles dans les melanges N2O4-HF que dans l'acide fluorhydrique. L'uranium dissous dans ces melanges est a l'etat pentavalent. Dans les melanges SbF5-HF l'uranium se dissout avec degagement d'hydrogene et passe a l'etat trivalent. Le compose solide resultant de la dissolution est un fluoantimoniate: U(SbF6)3. (auteur)

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Additional details

Additional titles

Original title (French)
Etude du comportement de quelques elements lourds dans des solvants a base d'acide fluorhydrique

Publishing Information

Imprint Pagination
[71 p.]
Report number
CEA-R--3205

Optional Information

Notes
66 refs.