Published October 8, 2004 | Version v1
Journal article

Comparative analysis of nanostructured diblock copolymer films

  • 1. Physik Department E13, TU Muenchen, James-Franck-Str. 1, 85748 Garching (Germany)
  • 2. Inst. fuer Polymerforschung Dresden e.V., Hohe Str. 6, 01069 Dresden (Germany)
  • 3. ESRF, BP 220, 38043 Grenoble Cedex (France)
  • 4. TU Muenchen, LS Physik Weihenstephan, Voettinger Strasse 40, 85350 Freising (Germany)
  • 5. HASYLAB at DESY, Notkestr. 85, 22603 Hamburg (Germany)

Description

Nanostructured polymer films of poly(styrene-block-paramethylstyrene) diblock copolymers P(Sd-b-pMS) on silicon substrates with a native oxide layer are investigated. Resulting from a storage under toluene vapor, a surface structure is installed. The early stages, characterized by the creation of a host structure out of an initially continuous film, are addressed. Grazing incidence small-angle X-ray scattering (GISAXS) experiments were performed as a function of exposure time. Results are compared to modelling of the scattering pattern and other experimental techniques, such as grazing incidence small-angle neutron scattering (GISANS) and atomic force microscopy (AFM) data. Possibilities and limits of the techniques are discussed

Additional details

Identifiers

DOI
10.1016/j.sab.2004.07.019;
PII
S0584-8547(04)00218-6;

Publishing Information

Journal Title
Spectrochimica Acta. Part B, Atomic Spectroscopy
Journal Volume
59
Journal Issue
10-11
Journal Page Range
p. 1789-1797
ISSN
0584-8547
CODEN
SAASBH

Conference

Title
17. International congress on X-ray optics and microanalysis
Dates
22-26 Sep 2003
Place
Chamonix (France)

Optional Information

Copyright
Copyright (c) 2004 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.